Technology Process of C17H25O3SN
There total 7 articles about C17H25O3SN which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
ethanol; water; toluene;
at 80 ℃;
for 0.75h;
DOI:10.1021/ol0713988
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine; 4-(dimethylamino)pyridine / CH2Cl2 / 2.5 h / 0 - 20 °C
2: CuBr*SMe2 / tetrahydrofuran; diethyl ether / -40 - -35 °C
3: sodium carbonate / Pd(Ph3P)4 / ethanol; toluene; H2O / 0.75 h / 80 °C
With
dmap; copper(I) bromide dimethylsulfide complex; sodium carbonate; triethylamine;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water; toluene;
2: Grignard reaction / 3: Suzuki coupling;
DOI:10.1021/ol0713988
- Guidance literature:
-
Multi-step reaction with 2 steps
1: CuBr*SMe2 / tetrahydrofuran; diethyl ether / -40 - -35 °C
2: sodium carbonate / Pd(Ph3P)4 / ethanol; toluene; H2O / 0.75 h / 80 °C
With
copper(I) bromide dimethylsulfide complex; sodium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; diethyl ether; ethanol; water; toluene;
1: Grignard reaction / 2: Suzuki coupling;
DOI:10.1021/ol0713988