3-azido-2-benzylpropyl benzyl ether

Base Information

Chemical Name:3-azido-2-benzylpropyl benzyl ether
CAS No.:332105-04-1
Molecular Formula:C₁₇H₁₉N₃O
Molecular Weight:281.357
Hs Code.:

Synonyms:3-azido-2-benzylpropyl benzyl ether

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Chemical Property of 3-azido-2-benzylpropyl benzyl ether

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Technology Process of 3-azido-2-benzylpropyl benzyl ether

There total 7 articles about 3-azido-2-benzylpropyl benzyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 100-39-0
benzyl bromide

: 289902-96-1,173216-46-1
3-azido-2-benzyl-1-propanol

: 332105-04-1
3-azido-2-benzylpropyl benzyl ether

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1016/S0968-0896(00)00216-9

Reference yield:

: 2612-30-8
2-benzyl-1,3-propanediol

: 332105-04-1
3-azido-2-benzylpropyl benzyl ether

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / p-toluenesulfonic acid / CH₂Cl₂ / 2 h / 20 °C

2: Et₃N / CH₂Cl₂ / 6 h / 20 °C

3: NaN₃ / dimethylformamide / 8 h / 80 °C

4: 98 percent / K₂CO₃ / methanol; H₂O / 2 h / 20 °C

5: 82 percent / NaH; Bu₄NI / tetrahydrofuran / 3 h / 20 °C

With sodium azide; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(00)00216-9

Reference yield:

: 90107-01-0
rac-2-hydroxymethyl-3-phenyl-propyl acetate

: 332105-04-1
3-azido-2-benzylpropyl benzyl ether

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / CH₂Cl₂ / 6 h / 20 °C

2: NaN₃ / dimethylformamide / 8 h / 80 °C

3: 98 percent / K₂CO₃ / methanol; H₂O / 2 h / 20 °C

4: 82 percent / NaH; Bu₄NI / tetrahydrofuran / 3 h / 20 °C

With sodium azide; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(00)00216-9