tert-butyl ((1R,2R)-3-hydroxy-1-phenyl-1-selenocyanatopropan-2-yl)carbamate

Base Information

Chemical Name:tert-butyl ((1R,2R)-3-hydroxy-1-phenyl-1-selenocyanatopropan-2-yl)carbamate
CAS No.:1377320-85-8
Molecular Formula:C₁₅H₂₀N₂O₃Se
Molecular Weight:355.295
Hs Code.:

Synonyms:tert-butyl ((1R,2R)-3-hydroxy-1-phenyl-1-selenocyanatopropan-2-yl)carbamate

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Chemical Property of tert-butyl ((1R,2R)-3-hydroxy-1-phenyl-1-selenocyanatopropan-2-yl)carbamate

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Technology Process of tert-butyl ((1R,2R)-3-hydroxy-1-phenyl-1-selenocyanatopropan-2-yl)carbamate

There total 1 articles about tert-butyl ((1R,2R)-3-hydroxy-1-phenyl-1-selenocyanatopropan-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1377320-84-7
(R)-tert-butyl 2,2-dimethyl-4-((R)-phenyl(selenocyanato)methyl)oxazolidine-3-carboxylate

: 1377320-85-8
tert-butyl ((1R,2R)-3-hydroxy-1-phenyl-1-selenocyanatopropan-2-yl)carbamate

Guidance literature:: With toluene-4-sulfonic acid; In 1,4-dioxane; at 20 ℃; for 4h;
DOI:10.1021/ol3012265

Reference yield: 71.0%

: 1377320-85-8
tert-butyl ((1R,2R)-3-hydroxy-1-phenyl-1-selenocyanatopropan-2-yl)carbamate

: 1377320-86-9
(2R,3R)-2-((tert-butoxycarbonyl)amino)-3-phenyl-3-selenocyanatopropanoic acid

Guidance literature:: With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; In water; acetonitrile; at 25 ℃; for 3h;
DOI:10.1021/acs.joc.9b02665

Reference yield:

: 1377320-85-8
tert-butyl ((1R,2R)-3-hydroxy-1-phenyl-1-selenocyanatopropan-2-yl)carbamate

: C₁₄H₁₉NO₄Se

Guidance literature:: Multi-step reaction with 2 steps

1: dipyridinium dichromate / N,N-dimethyl-formamide / 20 h / 20 °C

2: sodium tetrahydroborate / tetrahydrofuran; ethanol / 1 h / 0 °C

With sodium tetrahydroborate; dipyridinium dichromate; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/ol3012265