(R)-tert-butyl 2,2-dimethyl-4-((R)-phenyl(selenocyanato)methyl)oxazolidine-3-carboxylate

Base Information

Chemical Name:(R)-tert-butyl 2,2-dimethyl-4-((R)-phenyl(selenocyanato)methyl)oxazolidine-3-carboxylate
CAS No.:1377320-84-7
Molecular Formula:C₁₈H₂₄N₂O₃Se
Molecular Weight:395.36
Hs Code.:

Synonyms:(R)-tert-butyl 2,2-dimethyl-4-((R)-phenyl(selenocyanato)methyl)oxazolidine-3-carboxylate

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Chemical Property of (R)-tert-butyl 2,2-dimethyl-4-((R)-phenyl(selenocyanato)methyl)oxazolidine-3-carboxylate

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Technology Process of (R)-tert-butyl 2,2-dimethyl-4-((R)-phenyl(selenocyanato)methyl)oxazolidine-3-carboxylate

There total 1 articles about (R)-tert-butyl 2,2-dimethyl-4-((R)-phenyl(selenocyanato)methyl)oxazolidine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3425-46-5
potassium selenocyanate

: 124-63-0
methanesulfonyl chloride

: 1377320-84-7
(R)-tert-butyl 2,2-dimethyl-4-((R)-phenyl(selenocyanato)methyl)oxazolidine-3-carboxylate

Guidance literature:: In acetonitrile; at 45 ℃; for 20h;
DOI:10.1021/ol3012265

Reference yield: 75.0%

: 1377320-84-7
(R)-tert-butyl 2,2-dimethyl-4-((R)-phenyl(selenocyanato)methyl)oxazolidine-3-carboxylate

: 1377320-85-8
tert-butyl ((1R,2R)-3-hydroxy-1-phenyl-1-selenocyanatopropan-2-yl)carbamate

Guidance literature:: With toluene-4-sulfonic acid; In 1,4-dioxane; at 20 ℃; for 4h;
DOI:10.1021/ol3012265

Reference yield:

: 1377320-84-7
(R)-tert-butyl 2,2-dimethyl-4-((R)-phenyl(selenocyanato)methyl)oxazolidine-3-carboxylate

: 1377320-82-5
(2R,3R)-2-((tert-butoxycarbonyl)amino)-3-((4-methoxybenzyl)selanyl)-3-phenylpropanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: toluene-4-sulfonic acid / 1,4-dioxane / 4 h / 20 °C

2: dipyridinium dichromate / N,N-dimethyl-formamide / 20 h / 20 °C

3: sodium tetrahydroborate / tetrahydrofuran; ethanol / 1 h / 0 °C

4: sodium hydroxide / tetrahydrofuran; ethanol / 0 - 20 °C

With sodium tetrahydroborate; dipyridinium dichromate; toluene-4-sulfonic acid; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/ol3012265