5-bromo-2-methylphenylguanidine nitrate

Base Information

Chemical Name:5-bromo-2-methylphenylguanidine nitrate
CAS No.:1206604-19-4
Molecular Formula:C₈H₁₀BrN₃*HNO₃
Molecular Weight:291.104
Hs Code.:

Synonyms:5-bromo-2-methylphenylguanidine nitrate

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Chemical Property of 5-bromo-2-methylphenylguanidine nitrate

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Technology Process of 5-bromo-2-methylphenylguanidine nitrate

There total 2 articles about 5-bromo-2-methylphenylguanidine nitrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 5-bromo-2-methyl aniline hydrochloride

: 420-04-2
CYANAMID

: 1206604-19-4
5-bromo-2-methylphenylguanidine nitrate

Guidance literature:: 5-bromo-2-methyl aniline hydrochloride; CYANAMID; In tert-butyl alcohol; at 85 ℃; for 4h; Reflux;

With sodium hydroxide; In tert-butyl methyl ether; water; at 25 ℃; for 1h;

With nitric acid; at 12 ℃;

Reference yield: 79.9%

: 420-04-2
CYANAMID

: 39478-78-9
5-bromo-2-methylaniline

: 1206604-19-4
5-bromo-2-methylphenylguanidine nitrate

Guidance literature:: 5-bromo-2-methylaniline; With nitric acid; In methanol; at 60 ℃; for 0.5h;

CYANAMID; In methanol; water; for 6h; Reflux;
DOI:10.1021/acs.oprd.9b00227