N-(5-bromo-2-hydroxymethylphenyl)-N-(2-propenyl)-4-toluenesulfonylamide

Base Information

Chemical Name:N-(5-bromo-2-hydroxymethylphenyl)-N-(2-propenyl)-4-toluenesulfonylamide
CAS No.:223526-95-2
Molecular Formula:C₁₇H₁₈BrNO₃S
Molecular Weight:396.305
Hs Code.:

Synonyms:N-(5-bromo-2-hydroxymethylphenyl)-N-(2-propenyl)-4-toluenesulfonylamide

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Chemical Property of N-(5-bromo-2-hydroxymethylphenyl)-N-(2-propenyl)-4-toluenesulfonylamide

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Technology Process of N-(5-bromo-2-hydroxymethylphenyl)-N-(2-propenyl)-4-toluenesulfonylamide

There total 5 articles about N-(5-bromo-2-hydroxymethylphenyl)-N-(2-propenyl)-4-toluenesulfonylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 223526-94-1
methyl 5-bromo-2-(2-propenyl-4-toluenesulfonylamino)benzoate

: 223526-95-2
N-(5-bromo-2-hydroxymethylphenyl)-N-(2-propenyl)-4-toluenesulfonylamide

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃;
DOI:10.1016/S0040-4039(99)00150-1

Reference yield:

: 223526-84-9
methyl 5-bromo-2-{[(4-methylphenyl)sulfonyl]amino}benzoate

: 223526-95-2
N-(5-bromo-2-hydroxymethylphenyl)-N-(2-propenyl)-4-toluenesulfonylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / K₂CO₃ / acetone / 24 h / 20 °C

2: 68 percent / LiAlH₄ / tetrahydrofuran / 10 h / 0 °C

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; acetone;
DOI:10.1016/S0040-4020(01)00315-5

Reference yield:

: 52727-57-8
5-bromo-2-aminobenzoic acid methyl ester

: 223526-95-2
N-(5-bromo-2-hydroxymethylphenyl)-N-(2-propenyl)-4-toluenesulfonylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / pyridine / 40 h / 20 °C

2: 94 percent / K₂CO₃ / acetone / 24 h / 20 °C

3: 68 percent / LiAlH₄ / tetrahydrofuran / 10 h / 0 °C

With pyridine; lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; acetone;
DOI:10.1016/S0040-4020(01)00315-5