methyl 5-bromo-2-{[(4-methylphenyl)sulfonyl]amino}benzoate

Base Information

Chemical Name:methyl 5-bromo-2-{[(4-methylphenyl)sulfonyl]amino}benzoate
CAS No.:223526-84-9
Molecular Formula:C₁₅H₁₄BrNO₄S
Molecular Weight:384.25
Hs Code.:
Mol file:223526-84-9.mol

Synonyms:methyl 5-bromo-2-{[(4-methylphenyl)sulfonyl]amino}benzoate

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Chemical Property of methyl 5-bromo-2-{[(4-methylphenyl)sulfonyl]amino}benzoate

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Technology Process of methyl 5-bromo-2-{[(4-methylphenyl)sulfonyl]amino}benzoate

There total 3 articles about methyl 5-bromo-2-{[(4-methylphenyl)sulfonyl]amino}benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 50998-74-8
methyl N-tosylanthranilate

: 98-59-9
p-toluenesulfonyl chloride

: 223526-84-9
methyl 5-bromo-2-{[(4-methylphenyl)sulfonyl]amino}benzoate

Guidance literature:: With bromine; sodium acetate; In water; acetic acid; at 70 ℃; for 2h;

Reference yield: 94.0%

: 98-59-9
p-toluenesulfonyl chloride

: 52727-57-8
5-bromo-2-aminobenzoic acid methyl ester

: 223526-84-9
methyl 5-bromo-2-{[(4-methylphenyl)sulfonyl]amino}benzoate

Guidance literature:: With pyridine; at 20 ℃; for 40h;
DOI:10.1016/S0040-4020(01)00315-5

Reference yield:

: 134-20-3
2-carbomethoxyaniline

: 98-59-9
p-toluenesulfonyl chloride

: 223526-84-9
methyl 5-bromo-2-{[(4-methylphenyl)sulfonyl]amino}benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / tetrahydrofuran / 14.5 h / 20 °C

2: bromine; sodium acetate / water; acetic acid / 2 h / 70 °C

With pyridine; bromine; sodium acetate; In tetrahydrofuran; water; acetic acid;