1-S-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-mercaptopropionic acid pentafluorophenyl ester

Base Information

Chemical Name:1-S-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-mercaptopropionic acid pentafluorophenyl ester
CAS No.:850647-50-6
Molecular Formula:C₂₃H₂₃F₅O₁₁S
Molecular Weight:602.487
Hs Code.:

Synonyms:1-S-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-mercaptopropionic acid pentafluorophenyl ester

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Chemical Property of 1-S-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-mercaptopropionic acid pentafluorophenyl ester

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Technology Process of 1-S-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-mercaptopropionic acid pentafluorophenyl ester

There total 2 articles about 1-S-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-mercaptopropionic acid pentafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 25878-60-8
D-galactose pentaacetate

: 850647-50-6
1-S-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-mercaptopropionic acid pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / BF₃*OEt₂ / CH₂Cl₂ / 4 h / 20 °C

2: N,N'-diisopropylcarbodiimide / tetrahydrofuran / 24 h

With boron trifluoride diethyl etherate; diisopropyl-carbodiimide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm040794i

Reference yield:

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 79360-05-7
3-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-1-thio)propionic acid

: 850647-50-6
1-S-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-mercaptopropionic acid pentafluorophenyl ester

Guidance literature:: With diisopropyl-carbodiimide; In tetrahydrofuran; for 24h;
DOI:10.1021/jm040794i

Reference yield:

: 850647-50-6
1-S-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-mercaptopropionic acid pentafluorophenyl ester

: DOTAGA-(l-y)fk-(S)-Asu(NH₂)-KuE

: C₇₂H₁₀₇IN₁₂O₂₉S

Guidance literature:: 1-S-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-mercaptopropionic acid pentafluorophenyl ester; DOTAGA-(l-y)fk-(S)-Asu(NH₂)-KuE; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;

With potassium cyanide; In methanol; at 20 ℃;