1,2,2-trimethyl-1-phenyldisilane

Base Information

Chemical Name:1,2,2-trimethyl-1-phenyldisilane
CAS No.:53490-54-3
Molecular Formula:C₉H₁₆Si₂
Molecular Weight:180.397
Hs Code.:

Synonyms:1,2,2-trimethyl-1-phenyldisilane

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Chemical Property of 1,2,2-trimethyl-1-phenyldisilane

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Technology Process of 1,2,2-trimethyl-1-phenyldisilane

There total 7 articles about 1,2,2-trimethyl-1-phenyldisilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 111544-68-4
1,2-dichloro-1-phenyl-1,2,2-trimethyldisilane

: 53490-54-3
1,2,2-trimethyl-1-phenyldisilane

Guidance literature:: With sodium; In methanol; toluene; benzene;

Reference yield:

: 556816-33-2
(R)-1,2,2-trimethyl-2-(4-methoxynaphth-1-yl)-1-(naphth-1-yl)-1-phenyldisilane

: 53490-54-3
1,2,2-trimethyl-1-phenyldisilane

Guidance literature:: (R)-1,2,2-trimethyl-2-(4-methoxynaphth-1-yl)-1-(naphth-1-yl)-1-phenyldisilane; With trifluorormethanesulfonic acid; In chloroform; at -64 ℃;

With lithium aluminium tetrahydride; In diethyl ether; at 0 ℃;
DOI:10.1021/jo049398y

Reference yield:

: 69858-22-6
(R)-fluoro[methyl(naphth-1-yl)phenyl]silane

: 53490-54-3
1,2,2-trimethyl-1-phenyldisilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: MeLi / diethyl ether; tetrahydrofuran / -78 °C

1.2: tetrahydrofuran; diethyl ether / 1 h / 20 °C

2.1: triflic acid / CHCl₃ / -64 °C

2.2: LiAlH₄ / diethyl ether / 0 °C

With trifluorormethanesulfonic acid; methyllithium; In tetrahydrofuran; diethyl ether; chloroform;
DOI:10.1021/jo049398y