(R)-1,2,2-trimethyl-2-(4-methoxynaphth-1-yl)-1-(naphth-1-yl)-1-phenyldisilane

Base Information

Chemical Name:(R)-1,2,2-trimethyl-2-(4-methoxynaphth-1-yl)-1-(naphth-1-yl)-1-phenyldisilane
CAS No.:556816-33-2
Molecular Formula:C₃₀H₃₀OSi₂
Molecular Weight:462.739
Hs Code.:

Synonyms:(R)-1,2,2-trimethyl-2-(4-methoxynaphth-1-yl)-1-(naphth-1-yl)-1-phenyldisilane

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Chemical Property of (R)-1,2,2-trimethyl-2-(4-methoxynaphth-1-yl)-1-(naphth-1-yl)-1-phenyldisilane

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Technology Process of (R)-1,2,2-trimethyl-2-(4-methoxynaphth-1-yl)-1-(naphth-1-yl)-1-phenyldisilane

There total 4 articles about (R)-1,2,2-trimethyl-2-(4-methoxynaphth-1-yl)-1-(naphth-1-yl)-1-phenyldisilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 960-82-7
S(-)-methyl-α-naphthyl-phenyl-chlorosilane

: dimethyl(4-methoxynaphth-1-yl)silyltrimethylstannane

: 556816-33-2
(R)-1,2,2-trimethyl-2-(4-methoxynaphth-1-yl)-1-(naphth-1-yl)-1-phenyldisilane

Guidance literature:: dimethyl(4-methoxynaphth-1-yl)silyltrimethylstannane; With methyllithium; In tetrahydrofuran; diethyl ether; at -78 ℃;

S(-)-methyl-α-naphthyl-phenyl-chlorosilane; In tetrahydrofuran; pentane; at -78 ℃; for 1h;
DOI:10.1021/jo049398y

Reference yield:

: 69858-22-6
(R)-fluoro[methyl(naphth-1-yl)phenyl]silane

: dimethyl(4-methoxynaphth-1-yl)silyltrimethylstannane

: 556816-33-2
(R)-1,2,2-trimethyl-2-(4-methoxynaphth-1-yl)-1-(naphth-1-yl)-1-phenyldisilane

: (S)-1,2,2-trimethyl-2-(4-methoxynaphth-1-yl)-1-(naphth-1-yl)-1-phenyldisilane

Guidance literature:: dimethyl(4-methoxynaphth-1-yl)silyltrimethylstannane; With methyllithium; In tetrahydrofuran; diethyl ether; at -78 ℃;

(R)-fluoro[methyl(naphth-1-yl)phenyl]silane; In tetrahydrofuran; diethyl ether; at 20 ℃; for 1h; Title compound not separated from byproducts;
DOI:10.1021/jo049398y

Reference yield:

: 960-81-6
(S)-bromo[methyl(naphth-1-yl)phenyl]silane

: dimethyl(4-methoxynaphth-1-yl)silyltrimethylstannane

: 556816-33-2
(R)-1,2,2-trimethyl-2-(4-methoxynaphth-1-yl)-1-(naphth-1-yl)-1-phenyldisilane

: (S)-1,2,2-trimethyl-2-(4-methoxynaphth-1-yl)-1-(naphth-1-yl)-1-phenyldisilane

Guidance literature:: dimethyl(4-methoxynaphth-1-yl)silyltrimethylstannane; With methyllithium; In tetrahydrofuran; diethyl ether; at -78 ℃;

(S)-bromo[methyl(naphth-1-yl)phenyl]silane; In tetrahydrofuran; pentane; at -78 ℃; for 1h; Title compound not separated from byproducts;
DOI:10.1021/jo049398y