C₂₂H₂₇NO₄

Base Information

Chemical Name:C₂₂H₂₇NO₄
CAS No.:1395688-01-3
Molecular Formula:C₂₂H₂₇NO₄
Molecular Weight:369.461
Hs Code.:

C<sub>22</sub>H<sub>27</sub>NO<sub>4</sub>

Synonyms:C₂₂H₂₇NO₄

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Chemical Property of C₂₂H₂₇NO₄

Chemical Property:

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Technology Process of C₂₂H₂₇NO₄

There total 9 articles about C₂₂H₂₇NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1416404-30-2
C₁₉H₂₅NO₃

: 814-68-6,25189-84-8
acryloyl chloride

: 1395688-01-3
C₂₂H₂₇NO₄

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1021/jo302362b

Reference yield:

: 1395687-54-3
(R)-1-allyl-5-(benzyloxy)piperidin-2-one

: 1395688-01-3
C₂₂H₂₇NO₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: trifluoromethylsulfonic anhydride; 2,6-di-tert-butyl-4-methylpyridine / dichloromethane

2.1: lithium naphthalenide / tetrahydrofuran / 1 h / -40 °C

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C

4.1: hydrogenchloride / tetrahydrofuran; water / 1.5 h / 20 - 50 °C

4.3: CSA / 0.17 h / 90 °C

5.1: sodium hydride; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 18 h / 20 °C

6.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 1 h / 20 °C

7.1: triethylamine / dichloromethane / 0.5 h / 0 °C

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,6-di-tert-butyl-4-methylpyridine; oxalyl dichloride; trifluoromethylsulfonic anhydride; tetra-(n-butyl)ammonium iodide; sodium hydride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; 3.1: |Swern Oxidation / 3.2: |Swern Oxidation;
DOI:10.1021/jo302362b

Reference yield:

: 1395687-62-3
(2R,5R)-2-[2-(1,3-dioxolan-2-yl)ethyl]-1-allyl-5-(benzyloxy)-2-vinylpiperidine

: 1395688-01-3
C₂₂H₂₇NO₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: lithium naphthalenide / tetrahydrofuran / 1 h / -40 °C

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C

3.1: hydrogenchloride / tetrahydrofuran; water / 1.5 h / 20 - 50 °C

3.3: CSA / 0.17 h / 90 °C

4.1: sodium hydride; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 18 h / 20 °C

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 1 h / 20 °C

6.1: triethylamine / dichloromethane / 0.5 h / 0 °C

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; oxalyl dichloride; tetra-(n-butyl)ammonium iodide; sodium hydride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; 2.1: |Swern Oxidation / 2.2: |Swern Oxidation;
DOI:10.1021/jo302362b