2-{3-[(4-vinylbenzyloxy)methyl]-5-(tetrahydro-2H-pyran-2-yloxy)phenoxy}tetrahydro-2H-pyran

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Chemical Name:2-{3-[(4-vinylbenzyloxy)methyl]-5-(tetrahydro-2H-pyran-2-yloxy)phenoxy}tetrahydro-2H-pyran
CAS No.:858127-53-4
Molecular Formula:C₂₆H₃₂O₅
Molecular Weight:424.537
Hs Code.:

Synonyms:2-{3-[(4-vinylbenzyloxy)methyl]-5-(tetrahydro-2H-pyran-2-yloxy)phenoxy}tetrahydro-2H-pyran

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Chemical Property of 2-{3-[(4-vinylbenzyloxy)methyl]-5-(tetrahydro-2H-pyran-2-yloxy)phenoxy}tetrahydro-2H-pyran

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Technology Process of 2-{3-[(4-vinylbenzyloxy)methyl]-5-(tetrahydro-2H-pyran-2-yloxy)phenoxy}tetrahydro-2H-pyran

There total 3 articles about 2-{3-[(4-vinylbenzyloxy)methyl]-5-(tetrahydro-2H-pyran-2-yloxy)phenoxy}tetrahydro-2H-pyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 33617-42-4
(3,5-bis(tetrahydro-2H-pyran-2-yloxy)phenyl)methanol

: 1592-20-7,29296-32-0
4-Vinylbenzyl chloride

: 858127-53-4
2-{3-[(4-vinylbenzyloxy)methyl]-5-(tetrahydro-2H-pyran-2-yloxy)phenoxy}tetrahydro-2H-pyran

Guidance literature:: With 18-crown-6 ether; sodium hydride; In tetrahydrofuran; for 24h; Heating;
DOI:10.1021/ma047449n

Reference yield:

: 33617-41-3
3,5-bis(tetrahydropyran-2-yloxy)benzoic acid methyl ester

: 858127-53-4
2-{3-[(4-vinylbenzyloxy)methyl]-5-(tetrahydro-2H-pyran-2-yloxy)phenoxy}tetrahydro-2H-pyran

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / tetrahydrofuran / 4 h / Heating

2: 78 percent / sodium hydride; 18-crown-6 / tetrahydrofuran / 24 h / Heating

With lithium aluminium tetrahydride; 18-crown-6 ether; sodium hydride; In tetrahydrofuran; 2: Williamson reaction;
DOI:10.1021/ma047449n

Reference yield:

: 2150-44-9
1-carbomethoxy-3,5-dihydroxybenzene

: 858127-53-4
2-{3-[(4-vinylbenzyloxy)methyl]-5-(tetrahydro-2H-pyran-2-yloxy)phenoxy}tetrahydro-2H-pyran

Guidance literature:: Multi-step reaction with 3 steps

1: HCl / 48 h / 20 °C

2: LiAlH₄ / tetrahydrofuran / 4 h / Heating

3: 78 percent / sodium hydride; 18-crown-6 / tetrahydrofuran / 24 h / Heating

With hydrogenchloride; lithium aluminium tetrahydride; 18-crown-6 ether; sodium hydride; In tetrahydrofuran; 3: Williamson reaction;
DOI:10.1021/ma047449n