1-Aethyl-2-phenyl-3,3-dichlor-cyclobutenon

Base Information

• Chemical Name: 1-Aethyl-2-phenyl-3,3-dichlor-cyclobutenon
• CAS No.: 5909-89-7
• Molecular Formula: C₁₂H₁₀Cl₂O
• Molecular Weight: 241.117
• Mol file: 5909-89-7.mol

Synonyms:1-Aethyl-2-phenyl-3,3-dichlor-cyclobutenon

Chemical Property of 1-Aethyl-2-phenyl-3,3-dichlor-cyclobutenon

Chemical Property:

Purity/Quality:

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Technology Process of 1-Aethyl-2-phenyl-3,3-dichlor-cyclobutenon

There total 1 articles about 1-Aethyl-2-phenyl-3,3-dichlor-cyclobutenon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

1-phenyl-1-butyne (622-76-4,83585-27-7) + trifluoroacetyl chloride (76-02-8) → 1-Aethyl-2-phenyl-3,3-dichlor-cyclobutenon (5909-89-7)

Guidance literature:

With zinc; In 1,2-dimethoxyethane; diethyl ether; at 10 - 15 ℃; Irradiation;

DOI:10.1080/00397919508011825

Reference yield: 84.0%

1-Aethyl-2-phenyl-3,3-dichlor-cyclobutenon (5909-89-7) → 3-Ethyl-4-phenyl-3-cyclobuten-1,2-dione (17204-78-3)

Guidance literature:

With sulfuric acid; at 80 - 90 ℃; for 1h;

DOI:10.1080/00397919508011825

upstream raw materials:

1-phenyl-1-butyne

trifluoroacetyl chloride

Downstream raw materials:

3-Ethyl-4-phenyl-3-cyclobuten-1,2-dione