2-benzyloxy-4,6-dimethylphenacyl bromide

Base Information

Chemical Name:2-benzyloxy-4,6-dimethylphenacyl bromide
CAS No.:1265683-81-5
Molecular Formula:C₁₇H₁₇BrO₂
Molecular Weight:333.225
Hs Code.:

Synonyms:2-benzyloxy-4,6-dimethylphenacyl bromide

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Chemical Property of 2-benzyloxy-4,6-dimethylphenacyl bromide

Chemical Property:

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Technology Process of 2-benzyloxy-4,6-dimethylphenacyl bromide

There total 5 articles about 2-benzyloxy-4,6-dimethylphenacyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 1265683-72-4
2-benzyloxy-4,6-dimethylacetophenone

: 1265683-81-5
2-benzyloxy-4,6-dimethylphenacyl bromide

Guidance literature:: With copper(ll) bromide; In chloroform; ethyl acetate; at 80 ℃; for 2h;
DOI:10.1021/ol102887f

Reference yield:

: 108-68-9,50356-23-5
3,5-Dimethylphenol

: 1265683-81-5
2-benzyloxy-4,6-dimethylphenacyl bromide

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 0 - 20 °C

2: aluminum (III) chloride / nitromethane / 15 h / 0 - 50 °C

3: potassium carbonate / acetone / 24 h / Reflux

4: copper(ll) bromide / chloroform; ethyl acetate / 2 h / 80 °C

With aluminum (III) chloride; potassium carbonate; triethylamine; copper(ll) bromide; In nitromethane; dichloromethane; chloroform; ethyl acetate; acetone;
DOI:10.1021/ol102887f

Reference yield:

: 877-82-7
5-acetoxy-m-xylene

: 1265683-81-5
2-benzyloxy-4,6-dimethylphenacyl bromide

Guidance literature:: Multi-step reaction with 3 steps

1: aluminum (III) chloride / nitromethane / 15 h / 0 - 50 °C

2: potassium carbonate / acetone / 24 h / Reflux

3: copper(ll) bromide / chloroform; ethyl acetate / 2 h / 80 °C

With aluminum (III) chloride; potassium carbonate; copper(ll) bromide; In nitromethane; chloroform; ethyl acetate; acetone;
DOI:10.1021/ol102887f