(S)-4-((S)-4-Benzyloxycarbonyl-2-{2-[(R)-2-(2-benzyloxycarbonylamino-acetylamino)-3-mercapto-propionylamino]-acetylamino}-butyrylamino)-4-((S)-1,2-dicarbamoyl-ethylcarbamoyl)-butyric acid

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Chemical Name:(S)-4-((S)-4-Benzyloxycarbonyl-2-{2-[(R)-2-(2-benzyloxycarbonylamino-acetylamino)-3-mercapto-propionylamino]-acetylamino}-butyrylamino)-4-((S)-1,2-dicarbamoyl-ethylcarbamoyl)-butyric acid
CAS No.:80682-18-4
Molecular Formula:C₃₆H₄₆N₈O₁₃S
Molecular Weight:830.873
Hs Code.:

(S)-4-((S)-4-Benzyloxycarbonyl-2-{2-[(R)-2-(2-benzyloxycarbonylamino-acetylamino)-3-mercapto-propionylamino]-acetylamino}-butyrylamino)-4-((S)-1,2-dicarbamoyl-ethylcarbamoyl)-butyric acid

Synonyms:(S)-4-((S)-4-Benzyloxycarbonyl-2-{2-[(R)-2-(2-benzyloxycarbonylamino-acetylamino)-3-mercapto-propionylamino]-acetylamino}-butyrylamino)-4-((S)-1,2-dicarbamoyl-ethylcarbamoyl)-butyric acid

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Chemical Property of (S)-4-((S)-4-Benzyloxycarbonyl-2-{2-[(R)-2-(2-benzyloxycarbonylamino-acetylamino)-3-mercapto-propionylamino]-acetylamino}-butyrylamino)-4-((S)-1,2-dicarbamoyl-ethylcarbamoyl)-butyric acid

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Technology Process of (S)-4-((S)-4-Benzyloxycarbonyl-2-{2-[(R)-2-(2-benzyloxycarbonylamino-acetylamino)-3-mercapto-propionylamino]-acetylamino}-butyrylamino)-4-((S)-1,2-dicarbamoyl-ethylcarbamoyl)-butyric acid

There total 1 articles about (S)-4-((S)-4-Benzyloxycarbonyl-2-{2-[(R)-2-(2-benzyloxycarbonylamino-acetylamino)-3-mercapto-propionylamino]-acetylamino}-butyrylamino)-4-((S)-1,2-dicarbamoyl-ethylcarbamoyl)-butyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80682-17-3
C₇₂H₉₀N₁₆O₂₆S₂

: 80682-18-4
(S)-4-((S)-4-Benzyloxycarbonyl-2-{2-[(R)-2-(2-benzyloxycarbonylamino-acetylamino)-3-mercapto-propionylamino]-acetylamino}-butyrylamino)-4-((S)-1,2-dicarbamoyl-ethylcarbamoyl)-butyric acid

Guidance literature:: With tributylphosphine; In methanol; water; at 25 ℃; for 2h;
DOI:10.1021/ja00414a075

Reference yield:

: 80682-18-4
(S)-4-((S)-4-Benzyloxycarbonyl-2-{2-[(R)-2-(2-benzyloxycarbonylamino-acetylamino)-3-mercapto-propionylamino]-acetylamino}-butyrylamino)-4-((S)-1,2-dicarbamoyl-ethylcarbamoyl)-butyric acid

: 80682-20-8
3-[(3R,9S,12S)-3-(2-Benzyloxycarbonylamino-acetylamino)-12-((S)-1,2-dicarbamoyl-ethylcarbamoyl)-4,7,10,15-tetraoxo-1-thia-5,8,11-triaza-cyclopentadec-9-yl]-propionic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dicyclohexylcarbodiimide / dimethylformamide / 1.) 0 deg C, 1 h, 2.) 25 deg C, 18 h

2: triethylamine / tetrahydrofuran; dimethylformamide / 20 h / 40 °C

With triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ja00414a075

Reference yield:

: 2592-95-2
benzotriazol-1-ol

: 80682-18-4
(S)-4-((S)-4-Benzyloxycarbonyl-2-{2-[(R)-2-(2-benzyloxycarbonylamino-acetylamino)-3-mercapto-propionylamino]-acetylamino}-butyrylamino)-4-((S)-1,2-dicarbamoyl-ethylcarbamoyl)-butyric acid

: 80682-19-5
(S)-4-((S)-4-Benzyloxycarbonyl-2-{2-[(R)-2-(2-benzyloxycarbonylamino-acetylamino)-3-mercapto-propionylamino]-acetylamino}-butyrylamino)-4-((S)-1,2-dicarbamoyl-ethylcarbamoyl)-butyric acid benzotriazol-1-yl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; 1.) 0 deg C, 1 h, 2.) 25 deg C, 18 h;
DOI:10.1021/ja00414a075