(+)-(2S,3R)-cis-endo-2,3-bis(hydroxymethyl)bicyclo<2.2.1>heptane-2-carboxylic acid lactone

Base Information

Chemical Name:(+)-(2S,3R)-cis-endo-2,3-bis(hydroxymethyl)bicyclo<2.2.1>heptane-2-carboxylic acid lactone
CAS No.:95340-90-2
Molecular Formula:C₉H₁₂O₂
Molecular Weight:152.193
Hs Code.:

Synonyms:(+)-(2S,3R)-cis-endo-2,3-bis(hydroxymethyl)bicyclo<2.2.1>heptane-2-carboxylic acid lactone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-(2S,3R)-cis-endo-2,3-bis(hydroxymethyl)bicyclo<2.2.1>heptane-2-carboxylic acid lactone

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Technology Process of (+)-(2S,3R)-cis-endo-2,3-bis(hydroxymethyl)bicyclo<2.2.1>heptane-2-carboxylic acid lactone

There total 22 articles about (+)-(2S,3R)-cis-endo-2,3-bis(hydroxymethyl)bicyclo<2.2.1>heptane-2-carboxylic acid lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 95340-88-8
(3aS,4R,7S,7aR)-3a,4,7,7a-tetrahydro-4,7-methanoisobenzofuran-1(3H)-one

: 95340-90-2,694502-98-2
(+)-(2S,3R)-cis-endo-2,3-bis(hydroxymethyl)bicyclo<2.2.1>heptane-2-carboxylic acid lactone

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 2h; Ambient temperature;

Reference yield: 86.0%

: 5062-98-6
cis-endo-2,3-bis(hydroxymethyl)bicyclo<2.2.1>heptane

: 95340-90-2,694502-98-2
(+)-(2S,3R)-cis-endo-2,3-bis(hydroxymethyl)bicyclo<2.2.1>heptane-2-carboxylic acid lactone

Guidance literature:: With nicotinamide adenine dinucleotide; Flavin mononucleotide; HLADH; for 144h; Ambient temperature; 0.1 M NaOH-glycine buffer (pH=9);
DOI:10.1021/ja00294a052

Reference yield: 49.0%

: 5062-98-6
cis-endo-2,3-bis(hydroxymethyl)bicyclo<2.2.1>heptane

: 95340-90-2,694502-98-2
(+)-(2S,3R)-cis-endo-2,3-bis(hydroxymethyl)bicyclo<2.2.1>heptane-2-carboxylic acid lactone

: 694502-98-2
(2R,3S)-cis-endo-3-(hydroxymethyl)bicyclo[2.2.1]heptane-2-carboxylic acid lactone

Guidance literature:: With (1S,3R,4R)-1-(2-aza-bicyclo[2.2.1]hept-3-yl)methanol; [Cd*IrCl₂]2; potassium tert-butylate; In dichloromethane; acetone; at 20 ℃; for 48h;
DOI:10.1016/S0040-4039(03)00228-4