9-(4-chlorophenyl)-2-(3,4,5-tris(octadecyloxy)-cyclohexylmethoxy)-9-fluorenol

Base Information

Chemical Name:9-(4-chlorophenyl)-2-(3,4,5-tris(octadecyloxy)-cyclohexylmethoxy)-9-fluorenol
CAS No.:1245575-09-0
Molecular Formula:C₈₀H₁₃₃ClO₅
Molecular Weight:1210.39
Hs Code.:

Synonyms:9-(4-chlorophenyl)-2-(3,4,5-tris(octadecyloxy)-cyclohexylmethoxy)-9-fluorenol

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Chemical Property of 9-(4-chlorophenyl)-2-(3,4,5-tris(octadecyloxy)-cyclohexylmethoxy)-9-fluorenol

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Technology Process of 9-(4-chlorophenyl)-2-(3,4,5-tris(octadecyloxy)-cyclohexylmethoxy)-9-fluorenol

There total 4 articles about 9-(4-chlorophenyl)-2-(3,4,5-tris(octadecyloxy)-cyclohexylmethoxy)-9-fluorenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1245575-08-9
2-(3,4,5-tris(octadecyloxy)-cyclohexylmethoxy)-9-fluorenone

: 873-77-8
(4-chlorphenyl)magnesium bromide

: 1245575-09-0
9-(4-chlorophenyl)-2-(3,4,5-tris(octadecyloxy)-cyclohexylmethoxy)-9-fluorenol

Guidance literature:: 2-(3,4,5-tris(octadecyloxy)-cyclohexylmethoxy)-9-fluorenone; (4-chlorphenyl)magnesium bromide; In tetrahydrofuran; at 40 ℃; for 3h;

With hydrogenchloride; In water;

Reference yield:

: 1245575-07-8
3,4,5-tris(octadecyloxy)cyclohexylmethyl alcohol

: 1245575-09-0
9-(4-chlorophenyl)-2-(3,4,5-tris(octadecyloxy)-cyclohexylmethoxy)-9-fluorenol

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 1.5 h

2: tetrahydrofuran / 3 h / 40 °C

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran;

Reference yield:

: 1245575-06-7
methyl 3,4,5-tri(octadecyloxy)-cyclohexane carboxylate

: 1245575-09-0
9-(4-chlorophenyl)-2-(3,4,5-tris(octadecyloxy)-cyclohexylmethoxy)-9-fluorenol

Guidance literature:: Multi-step reaction with 3 steps

1: diisobutylaluminium hydride / tetrahydrofuran / 0.5 h / 20 °C

2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 1.5 h

3: tetrahydrofuran / 3 h / 40 °C

With diisobutylaluminium hydride; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran;