9-(4-chlorophenyl)-2-(3,4,5-tris(octadecyloxy)-cyclohexylmethoxy)-9-bromofluorene

Base Information

Chemical Name:9-(4-chlorophenyl)-2-(3,4,5-tris(octadecyloxy)-cyclohexylmethoxy)-9-bromofluorene
CAS No.:1245575-10-3
Molecular Formula:C₈₀H₁₃₂BrClO₄
Molecular Weight:1273.28
Hs Code.:

Synonyms:9-(4-chlorophenyl)-2-(3,4,5-tris(octadecyloxy)-cyclohexylmethoxy)-9-bromofluorene

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Chemical Property of 9-(4-chlorophenyl)-2-(3,4,5-tris(octadecyloxy)-cyclohexylmethoxy)-9-bromofluorene

Chemical Property:

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Technology Process of 9-(4-chlorophenyl)-2-(3,4,5-tris(octadecyloxy)-cyclohexylmethoxy)-9-bromofluorene

There total 4 articles about 9-(4-chlorophenyl)-2-(3,4,5-tris(octadecyloxy)-cyclohexylmethoxy)-9-bromofluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1245575-09-0
9-(4-chlorophenyl)-2-(3,4,5-tris(octadecyloxy)-cyclohexylmethoxy)-9-fluorenol

: 1245575-10-3
9-(4-chlorophenyl)-2-(3,4,5-tris(octadecyloxy)-cyclohexylmethoxy)-9-bromofluorene

Guidance literature:: With Acetyl bromide; In chloroform; at 20 ℃; for 1h;

Reference yield:

: 1245575-07-8
3,4,5-tris(octadecyloxy)cyclohexylmethyl alcohol

: 1245575-10-3
9-(4-chlorophenyl)-2-(3,4,5-tris(octadecyloxy)-cyclohexylmethoxy)-9-bromofluorene

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 1.5 h

2: tetrahydrofuran / 3 h / 40 °C

3: Acetyl bromide / chloroform / 1 h / 20 °C

With Acetyl bromide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; chloroform;

Reference yield:

: 1245575-06-7
methyl 3,4,5-tri(octadecyloxy)-cyclohexane carboxylate

: 1245575-10-3
9-(4-chlorophenyl)-2-(3,4,5-tris(octadecyloxy)-cyclohexylmethoxy)-9-bromofluorene

Guidance literature:: Multi-step reaction with 4 steps

1: diisobutylaluminium hydride / tetrahydrofuran / 0.5 h / 20 °C

2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 1.5 h

3: tetrahydrofuran / 3 h / 40 °C

4: Acetyl bromide / chloroform / 1 h / 20 °C

With Acetyl bromide; diisobutylaluminium hydride; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; chloroform;