tert-butyl N-benzyl-N-[1-(2-iodo-3-methoxyphenyl)-3-(3-methoxyphenyl)but-3-en-2-yl]carbamate

Base Information

Chemical Name:tert-butyl N-benzyl-N-[1-(2-iodo-3-methoxyphenyl)-3-(3-methoxyphenyl)but-3-en-2-yl]carbamate
CAS No.:1131444-96-6
Molecular Formula:C₃₀H₃₄INO₄
Molecular Weight:599.509
Hs Code.:

Synonyms:tert-butyl N-benzyl-N-[1-(2-iodo-3-methoxyphenyl)-3-(3-methoxyphenyl)but-3-en-2-yl]carbamate

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Chemical Property of tert-butyl N-benzyl-N-[1-(2-iodo-3-methoxyphenyl)-3-(3-methoxyphenyl)but-3-en-2-yl]carbamate

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Technology Process of tert-butyl N-benzyl-N-[1-(2-iodo-3-methoxyphenyl)-3-(3-methoxyphenyl)but-3-en-2-yl]carbamate

There total 1 articles about tert-butyl N-benzyl-N-[1-(2-iodo-3-methoxyphenyl)-3-(3-methoxyphenyl)but-3-en-2-yl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1131444-95-5
tert-butyl N-benzyl-N-[3-(2-iodo-3-methoxyphenyl)-1-(3-methoxyphenyl)-1-oxoprop-2-yl]carbamate

: 1779-49-3
Methyltriphenylphosphonium bromide

: 1131444-96-6
tert-butyl N-benzyl-N-[1-(2-iodo-3-methoxyphenyl)-3-(3-methoxyphenyl)but-3-en-2-yl]carbamate

Guidance literature:: Methyltriphenylphosphonium bromide; With potassium hexamethylsilazane; In tetrahydrofuran; at -78 ℃; for 0.25h;

tert-butyl N-benzyl-N-[3-(2-iodo-3-methoxyphenyl)-1-(3-methoxyphenyl)-1-oxoprop-2-yl]carbamate; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1021/jo802787j

Reference yield:

: 1131444-96-6
tert-butyl N-benzyl-N-[1-(2-iodo-3-methoxyphenyl)-3-(3-methoxyphenyl)but-3-en-2-yl]carbamate

: C₂₅H₂₆INO₂

Guidance literature:: tert-butyl N-benzyl-N-[1-(2-iodo-3-methoxyphenyl)-3-(3-methoxyphenyl)but-3-en-2-yl]carbamate; With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 1h;

With sodium hydrogencarbonate; In dichloromethane; water;
DOI:10.1021/jo802787j