4,4-difluoro-8-(3',5'-bis(decyloxy)phenyl)-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

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Chemical Name:4,4-difluoro-8-(3',5'-bis(decyloxy)phenyl)-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene
CAS No.:1094811-95-6
Molecular Formula:C₃₉H₅₉BF₂N₂O₂
Molecular Weight:636.717
Hs Code.:

Synonyms:4,4-difluoro-8-(3',5'-bis(decyloxy)phenyl)-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

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Chemical Property of 4,4-difluoro-8-(3',5'-bis(decyloxy)phenyl)-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

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Technology Process of 4,4-difluoro-8-(3',5'-bis(decyloxy)phenyl)-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

There total 1 articles about 4,4-difluoro-8-(3',5'-bis(decyloxy)phenyl)-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 259877-84-4
3,5-bis(decycloxy)benzaldehyde

: 625-82-1
2,4-dimethyl-1H-pyrrole

: 1094811-95-6
4,4-difluoro-8-(3',5'-bis(decyloxy)phenyl)-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: 3,5-bis(decycloxy)benzaldehyde; 2,4-dimethyl-1H-pyrrole; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; for 0.5h; Inert atmosphere;

With boron trifluoride diethyl etherate; triethylamine; In dichloromethane; for 0.5h; Inert atmosphere;
DOI:10.1021/ol802446e

Reference yield: 95.0%

: 1094811-95-6
4,4-difluoro-8-(3',5'-bis(decyloxy)phenyl)-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

: 1094812-00-6
4,4-difluoro-8-[3',5'-bis(decyloxy)phenyl]-2,6-diiodo-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: With iodine; iodic acid; In ethanol; water; at 60 ℃; for 1h;
DOI:10.1002/chem.200802538

Reference yield: 89.0%

: 1094811-95-6
4,4-difluoro-8-(3',5'-bis(decyloxy)phenyl)-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1243170-04-8
C₄₀H₅₉BF₂N₂O₃

Guidance literature:: N,N-dimethyl-formamide; With trichlorophosphate; at 20 ℃; Inert atmosphere; Cooling with ice;

4,4-difluoro-8-(3',5'-bis(decyloxy)phenyl)-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene; In 1,2-dichloro-ethane; at 20 - 50 ℃; Inert atmosphere;
DOI:10.1021/ol1014762