(C₅H₅)(CO)2Ru(P(C₆H₅)3)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)(CO)2Ru(P(C₆H₅)3)PF₆

Base Information

Chemical Name:(C₅H₅)(CO)2Ru(P(C₆H₅)3)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)(CO)2Ru(P(C₆H₅)3)PF₆
CAS No.:91482-99-4
Molecular Formula:C₂₅H₂₀O₂PRu*F₆P
Molecular Weight:629.441
Hs Code.:

(C<sub>5</sub>H<sub>5</sub>)(CO)2Ru(P(C<sub>6</sub>H<sub>5</sub>)3)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=(C<sub>5</sub>H<sub>5</sub>)(CO)2Ru(P(C<sub>6</sub>H<sub>5</sub>)3)PF<sub>6</sub>

Synonyms:(C₅H₅)(CO)2Ru(P(C₆H₅)3)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)(CO)2Ru(P(C₆H₅)3)PF₆

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Chemical Property of (C₅H₅)(CO)2Ru(P(C₆H₅)3)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)(CO)2Ru(P(C₆H₅)3)PF₆

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Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (C₅H₅)(CO)2Ru(P(C₆H₅)3)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)(CO)2Ru(P(C₆H₅)3)PF₆

There total 3 articles about (C₅H₅)(CO)2Ru(P(C₆H₅)3)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)(CO)2Ru(P(C₆H₅)3)PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: ammonium hexafluorophosphate

: 32613-25-5
[(η5-cyclopentadienyl)ruthenium(II)(triphenylphosphine)(carbonyl)(chloride)]

: 91482-99-4
(C₅H₅)(CO)2Ru(P(C₆H₅)3)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)(CO)2Ru(P(C₆H₅)3)PF₆

Guidance literature:: With carbon monoxide; In methanol; a suspn. of Ru-complex and NH4PF6 in MeOH was stirred (50°C) under CO (3 atm) for 10 h under N2; solvent was removed under reduced pressure, extd. with CH2Cl2, concd., Et2O was slowly added, cooled to -30°C;
DOI:10.1039/DT9840000993

Reference yield: 71.0%

: [C₅H₅RuP(C₆H₅)3(CO)C(OCH(CH₃)2)CH₂C₆H₅]⁽¹⁺⁾*PF₆^(1-)=[C₅H₅RuP(C₆H₅)3(CO)C(OCH(CH₃)2)CH₂C₆H₅]PF₆

: 91482-99-4
(C₅H₅)(CO)2Ru(P(C₆H₅)3)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)(CO)2Ru(P(C₆H₅)3)PF₆

Guidance literature:: In diethyl ether; High Pressure; heated in wet ether in a autoclave for 7 h at 60°C; cooled; evapd.; recrystd. (light petroleum/acetone); elem. anal.;

Reference yield:

: 4590-57-2
HPF₆*Et₂O

: Ru(C2Ph)(CO)(PPh3)(η-C5H5)

: 91482-99-4
(C₅H₅)(CO)2Ru(P(C₆H₅)3)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)(CO)2Ru(P(C₆H₅)3)PF₆

Guidance literature:: In dichloromethane; N2, excess HPf6*OET2 added slowly to a soln. of Ru-complex in CH2Cl2 with water, 1,5 h at room temp., heated for 24 h; IR;