2-Acetyl-1-(p-bromophenyl)-1-methylhydrazine

Base Information

Chemical Name:2-Acetyl-1-(p-bromophenyl)-1-methylhydrazine
CAS No.:90560-93-3
Molecular Formula:C₉H₁₁BrN₂O
Molecular Weight:243.103
Hs Code.:
DSSTox Substance ID:DTXSID301236998
Nikkaji Number:J1.424.591J

Synonyms:DTXSID301236998;2'-(p-Bromophenyl)-2'-methylacetohydrazide;2-Acetyl-1-(p-bromophenyl)-1-methylhydrazine;N'-(4-Bromophenyl)-N'-methylacetohydrazide #;Acetic acid, 2-(4-bromophenyl)-2-methylhydrazide;90560-93-3

Suppliers and Price of 2-Acetyl-1-(p-bromophenyl)-1-methylhydrazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 2-Acetyl-1-(p-bromophenyl)-1-methylhydrazine

Chemical Property:

XLogP3:2.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:242.00548
Heavy Atom Count:13
Complexity:179

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)NN(C)C1=CC=C(C=C1)Br

Technology Process of 2-Acetyl-1-(p-bromophenyl)-1-methylhydrazine

There total 3 articles about 2-Acetyl-1-(p-bromophenyl)-1-methylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 14579-97-6
2-acetyl-1-(4-bromophenyl)hydrazine

: 74-88-4
methyl iodide

: 90560-93-3
N'-(4-bromophenyl)-N'-methylacetohydrazide

Guidance literature:: With sodium; In ethanol; at 100 ℃; for 20h; Sealed tube; Darkness;
DOI:10.1002/anie.201207173

Reference yield:

: 589-21-9
(4-bromophenyl)hydrazine

: 90560-93-3
N'-(4-bromophenyl)-N'-methylacetohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.5 h / 20 - 80 °C / Inert atmosphere

2: sodium / ethanol / 20 h / 100 °C / Sealed tube; Darkness

With sodium; In ethanol;
DOI:10.1002/anie.201207173