4-methoxy-2-trimethylsilylphenyl diethylphosphate

Base Information

Chemical Name:4-methoxy-2-trimethylsilylphenyl diethylphosphate
CAS No.:1366440-94-9
Molecular Formula:C₁₄H₂₅O₅PSi
Molecular Weight:332.409
Hs Code.:

Synonyms:4-methoxy-2-trimethylsilylphenyl diethylphosphate

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Chemical Property of 4-methoxy-2-trimethylsilylphenyl diethylphosphate

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Technology Process of 4-methoxy-2-trimethylsilylphenyl diethylphosphate

There total 4 articles about 4-methoxy-2-trimethylsilylphenyl diethylphosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 85630-29-1
4-methoxy-2-trimethylsilylphenol

: 814-49-3
diethyl chlorophosphate

: 1366440-94-9
4-methoxy-2-trimethylsilylphenyl diethylphosphate

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 3h;
DOI:10.1021/jo300290v

Reference yield:

: 1366440-80-3
4-methoxy-2-trimethylsilylphenyl methanesulfonate

: 1366440-94-9
4-methoxy-2-trimethylsilylphenyl diethylphosphate

Guidance literature:: Multi-step reaction with 2 steps

1: water; acetone / 12 h / Photolysis

2: sodium hydride / tetrahydrofuran / 3 h / 0 - 20 °C

With water; sodium hydride; acetone; In tetrahydrofuran;
DOI:10.1021/jo300290v

Reference yield:

: 1004322-70-6
2-chloro-5-methoxyphenyltrimethylsilane

: 1366440-94-9
4-methoxy-2-trimethylsilylphenyl diethylphosphate

Guidance literature:: Multi-step reaction with 2 steps

1: water; acetone / 25 h / Photolysis

2: sodium hydride / tetrahydrofuran / 3 h / 0 - 20 °C

With water; sodium hydride; acetone; In tetrahydrofuran;
DOI:10.1021/jo300290v