C₅₅H₅₂O₁₅

Base Information

Chemical Name:C₅₅H₅₂O₁₅
CAS No.:203717-61-7
Molecular Formula:C₅₅H₅₂O₁₅
Molecular Weight:953.009
Hs Code.:

C<sub>55</sub>H<sub>52</sub>O<sub>15</sub>

Synonyms:C₅₅H₅₂O₁₅

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Chemical Property of C₅₅H₅₂O₁₅

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Technology Process of C₅₅H₅₂O₁₅

There total 5 articles about C₅₅H₅₂O₁₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14218-11-2
2,3,4,6-tetra-O-benzoylglucosyl bromide

: 203717-61-7
C₅₅H₅₂O₁₅

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / AgOTf, s-collidine, molecular sieves 4A / CH₂Cl₂ / 2 h / -30 °C

2: tris(triphenylphosphine)rhodium(I) chloride, diisopropylethylamine / ethanol / 3 h / Heating

3: toluene-p-sulfonic acid

With 2,4,6-trimethyl-pyridine; Wilkinson's catalyst; 4 A molecular sieve; silver trifluoromethanesulfonate; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane;
DOI:10.1039/a707346a

Reference yield:

: 58341-59-6
methyl 2,6-di-O-benzyl-3-O-allyl-α-D-glucopyranoside

: 203717-61-7
C₅₅H₅₂O₁₅

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / AgOTf, s-collidine, molecular sieves 4A / CH₂Cl₂ / 2 h / -30 °C

2: tris(triphenylphosphine)rhodium(I) chloride, diisopropylethylamine / ethanol / 3 h / Heating

3: toluene-p-sulfonic acid

With 2,4,6-trimethyl-pyridine; Wilkinson's catalyst; 4 A molecular sieve; silver trifluoromethanesulfonate; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane;
DOI:10.1039/a707346a

Reference yield:

: 76375-66-1
methyl 2-O-benzyl-4,6-O-benzylidene-α-D-glucopyranoside

: 203717-61-7
C₅₅H₅₂O₁₅

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / NaH / dimethylformamide / 1 h / Ambient temperature

2: 1.) NaCNBH₃, 2.) HCl / 1.) THF, room temperature, 0.5 h, 2.) diethyl ether

3: 74 percent / AgOTf, s-collidine, molecular sieves 4A / CH₂Cl₂ / 2 h / -30 °C

4: tris(triphenylphosphine)rhodium(I) chloride, diisopropylethylamine / ethanol / 3 h / Heating

5: toluene-p-sulfonic acid

With 2,4,6-trimethyl-pyridine; hydrogenchloride; Wilkinson's catalyst; 4 A molecular sieve; silver trifluoromethanesulfonate; sodium hydride; sodium cyanoborohydride; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/a707346a