N-<<(1S,2R,3R,5S)-2,6,6-trimethylbicyclo<3.1.1>hept-3-yl>methyl>-2,2,2-trifluoro-1,1-diphenylethanesulfenamide

Base Information

• Chemical Name: N-<<(1S,2R,3R,5S)-2,6,6-trimethylbicyclo<3.1.1>hept-3-yl>methyl>-2,2,2-trifluoro-1,1-diphenylethanesulfenamide
• CAS No.: 138036-47-2
• Molecular Formula: C₂₅H₃₀F₃NS
• Molecular Weight: 433.581
• Mol file: 138036-47-2.mol

Synonyms:N-<<(1S,2R,3R,5S)-2,6,6-trimethylbicyclo<3.1.1>hept-3-yl>methyl>-2,2,2-trifluoro-1,1-diphenylethanesulfenamide

Chemical Property of N-<<(1S,2R,3R,5S)-2,6,6-trimethylbicyclo<3.1.1>hept-3-yl>methyl>-2,2,2-trifluoro-1,1-diphenylethanesulfenamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-<<(1S,2R,3R,5S)-2,6,6-trimethylbicyclo<3.1.1>hept-3-yl>methyl>-2,2,2-trifluoro-1,1-diphenylethanesulfenamide

There total 1 articles about N-<<(1S,2R,3R,5S)-2,6,6-trimethylbicyclo<3.1.1>hept-3-yl>methyl>-2,2,2-trifluoro-1,1-diphenylethanesulfenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

2,2,2-trifluoro-1,1-diphenylethane-sulfenyl chloride (112881-92-2) + (+)-3-(aminomethyl)pinane hydrochloride (57357-84-3) → N-<<(1S,2R,3R,5S)-2,6,6-trimethylbicyclo<3.1.1>hept-3-yl>methyl>-2,2,2-trifluoro-1,1-diphenylethanesulfenamide (138036-47-2)

Guidance literature:

With sodium carbonate; In tetrahydrofuran; for 0.0833333h;

DOI:10.1016/S0040-4020(01)91009-9

Reference yield: 95.0%

N-<<(1S,2R,3R,5S)-2,6,6-trimethylbicyclo<3.1.1>hept-3-yl>methyl>-2,2,2-trifluoro-1,1-diphenylethanesulfenamide (138036-47-2) → 2,2,2-trifluoro-1,1-diphenylethane-sulfenyl chloride (112881-92-2) + (+)-3-(aminomethyl)pinane hydrochloride (57357-84-3)

Guidance literature:

With hydrogenchloride; In diethyl ether; Product distribution; Ambient temperature; other in the same manner protected amines investigated;

DOI:10.1016/S0040-4020(01)91009-9

upstream raw materials:

2,2,2-trifluoro-1,1-diphenylethane-sulfenyl chloride

(+)-3-(aminomethyl)pinane hydrochloride

Downstream raw materials:

2,2,2-trifluoro-1,1-diphenylethane-sulfenyl chloride

(+)-3-(aminomethyl)pinane hydrochloride