(2R,3S)-2,3-piperidinedicarboxylic acid dimethyl ester

Base Information

Chemical Name:(2R,3S)-2,3-piperidinedicarboxylic acid dimethyl ester
CAS No.:149880-78-4
Molecular Formula:C₉H₁₅NO₄
Molecular Weight:201.222
Hs Code.:

Synonyms:(2R,3S)-2,3-piperidinedicarboxylic acid dimethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3S)-2,3-piperidinedicarboxylic acid dimethyl ester

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Technology Process of (2R,3S)-2,3-piperidinedicarboxylic acid dimethyl ester

There total 8 articles about (2R,3S)-2,3-piperidinedicarboxylic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 605-38-9
dimethyl 2,3-pyridinedicarboxylate

: 23513-23-7,23580-75-8,40740-62-3,138738-48-4,149880-78-4
cis-(±)-dimethyl piperidine-2,3-dicarboxylate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In toluene; at 50 - 60 ℃; for 5h; under 7500.75 Torr; Autoclave;

Reference yield: 57.0%

: 605-38-9
dimethyl 2,3-pyridinedicarboxylate

: 23513-23-7,23580-75-8,40740-62-3,138738-48-4,149880-78-4
trans-dimethyl piperidine-2,3-dicarboxylate

: 23513-23-7,23580-75-8,40740-62-3,138738-48-4,149880-78-4
cis-(±)-dimethyl piperidine-2,3-dicarboxylate

Guidance literature:: With Adam’s catalyst; hydrogen; acetic acid; for 6h; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/jacs.5b07201

Reference yield: 57.0%

: 605-38-9
dimethyl 2,3-pyridinedicarboxylate

: 23513-23-7,23580-75-8,40740-62-3,138738-48-4,149880-78-4
trans-dimethyl piperidine-2,3-dicarboxylate

: 23513-23-7,23580-75-8,40740-62-3,138738-48-4,149880-78-4
cis-(±)-dimethyl piperidine-2,3-dicarboxylate

Guidance literature:: With Adam’s catalyst; hydrogen; acetic acid; for 6h; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/jacs.5b07201