2--1-(p-tolylsulfonyl)hydrazine

Base Information

Chemical Name:2--1-(p-tolylsulfonyl)hydrazine
CAS No.:74618-09-0
Molecular Formula:C₁₇H₁₈N₂O₄S
Molecular Weight:346.407
Hs Code.:

2-<o-(allyloxy)-benzoyl>-1-(p-tolylsulfonyl)hydrazine

Synonyms:2--1-(p-tolylsulfonyl)hydrazine

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Chemical Property of 2--1-(p-tolylsulfonyl)hydrazine

Chemical Property:

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Technology Process of 2--1-(p-tolylsulfonyl)hydrazine

There total 5 articles about 2--1-(p-tolylsulfonyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 52542-42-4
2-allyloxybenzoyl chloride

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 74618-09-0
2--1-(p-tolylsulfonyl)hydrazine

Guidance literature:: With triethylamine; In benzene; for 3h; Heating;
DOI:10.1246/bcsj.53.429

Reference yield: 56.0%

: 74618-13-6
1-acetyl-2-(o-allyloxy)benzoyl-1-p-tolylsulfonylhydrazine

: 74618-09-0
2--1-(p-tolylsulfonyl)hydrazine

Guidance literature:: With potassium hydroxide; In ethanol; for 1h; Heating;
DOI:10.1246/bcsj.53.429

Reference yield:

: 6282-42-4
methyl 2-allyloxybenzoate

: 74618-09-0
2--1-(p-tolylsulfonyl)hydrazine

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / aq. NaOH / aq. ethanol / Heating

2: thionyl chloride

3: 57 percent / Et₃N / benzene / 3 h / Heating

With sodium hydroxide; thionyl chloride; triethylamine; In ethanol; benzene;
DOI:10.1246/bcsj.53.429