2-(4-chlorophenyl)-5-{(1E,3Z)-3-[methyl(oxido)imino]prop-1-en-1-yl}-2H-tetrazole

Base Information

• Chemical Name: 2-(4-chlorophenyl)-5-{(1E,3Z)-3-[methyl(oxido)imino]prop-1-en-1-yl}-2H-tetrazole
• CAS No.: 802910-91-4
• Molecular Formula: C₁₁H₁₀ClN₅O
• Molecular Weight: 263.686

Synonyms:2-(4-chlorophenyl)-5-{(1E,3Z)-3-[methyl(oxido)imino]prop-1-en-1-yl}-2H-tetrazole

Chemical Property of 2-(4-chlorophenyl)-5-{(1E,3Z)-3-[methyl(oxido)imino]prop-1-en-1-yl}-2H-tetrazole

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Technology Process of 2-(4-chlorophenyl)-5-{(1E,3Z)-3-[methyl(oxido)imino]prop-1-en-1-yl}-2H-tetrazole

There total 1 articles about 2-(4-chlorophenyl)-5-{(1E,3Z)-3-[methyl(oxido)imino]prop-1-en-1-yl}-2H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

N-methylhydroxyamine hydrochloride (4229-44-1) + 2-(4-chlorophenyl)-5-[(1E)-3-oxoprop-1-en-1-yl]-2H-tetrazole (670276-69-4) → 2-(4-chlorophenyl)-5-{(1E,3Z)-3-[methyl(oxido)imino]prop-1-en-1-yl}-2H-tetrazole (802910-91-4)

Guidance literature:

With sodium acetate; In ethanol; at 20 ℃;

DOI:10.3987/com-04-10158

Reference yield: 61.0%

Phenyl[2-(trimethylsilyl)phenyl]iodonium trifluoromethanesulfonate (164594-13-2) + 2-(4-chlorophenyl)-5-{(1E,3Z)-3-[methyl(oxido)imino]prop-1-en-1-yl}-2H-tetrazole (802910-91-4) → 3-{(E)-2-[2-(4-chlorophenyl)-2H-tetrazol-5-yl]vinyl}-2-methyl-2,3-dihydro-1,2-benzisoxazole

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane; at 0 ℃; for 1h;

DOI:10.3987/com-04-10158

Reference yield: 39.0%

N-methylmaleimide (930-88-1) + 2-(4-chlorophenyl)-5-{(1E,3Z)-3-[methyl(oxido)imino]prop-1-en-1-yl}-2H-tetrazole (802910-91-4) → (3S,3aS,6aR)-3-{(E)-2-[2-(4-chlorophenyl)-2H-tetrazol-5-yl]vinyl}-2,5-dimethyldihydro-2H-pyrrolo[3,4-d]isoxazole-4,6(3H,5H)-dione + (3R,3aS,6aR)-3-{(E)-2-[2-(4-chlorophenyl)-2H-tetrazol-5-yl]vinyl}-2,5-dimethyldihydro-2H-pyrrolo[3,4-d]isoxazole-4,6(3H,5H)-dione

Guidance literature:

In toluene; for 27.5h; Heating;

DOI:10.3987/com-04-10158

upstream raw materials:

N-methylhydroxyamine hydrochloride

2-(4-chlorophenyl)-5-[(1E)-3-oxoprop-1-en-1-yl]-2H-tetrazole

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