C₄₇H₅₉ClN₄O₆SSi

Base Information

Chemical Name:C₄₇H₅₉ClN₄O₆SSi
CAS No.:1380213-66-0
Molecular Formula:C₄₇H₅₉ClN₄O₆SSi
Molecular Weight:871.613
Hs Code.:

C<sub>47</sub>H<sub>59</sub>ClN<sub>4</sub>O<sub>6</sub>SSi

Synonyms:C₄₇H₅₉ClN₄O₆SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₇H₅₉ClN₄O₆SSi

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Technology Process of C₄₇H₅₉ClN₄O₆SSi

There total 7 articles about C₄₇H₅₉ClN₄O₆SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1380213-61-5
2-chloro-1-methyltryptamine nosylamide

: 1380213-65-9
C₃₀H₄₄ClNO₂Si

: 1380213-66-0
C₄₇H₅₉ClN₄O₆SSi

Guidance literature:: With tetra-(n-butyl)ammonium iodide; potassium hydride; In N,N-dimethyl-formamide; at 23 - 100 ℃; for 24.0833h; Inert atmosphere;
DOI:10.1002/anie.201200387

Reference yield:

: 1380213-63-7
C₁₉H₂₁NO₂

: 1380213-66-0
C₄₇H₅₉ClN₄O₆SSi

Guidance literature:: Multi-step reaction with 4 steps

1.1: 2,2,6,6-tetramethylpiperidinyl-lithium; lithium chloride / tetrahydrofuran; hexane / 0.33 h / -78 - 0 °C

1.2: 5.17 h / -78 - 0 °C / Inert atmosphere

2.1: lithium chloride; lithium diisopropyl amide / tetrahydrofuran; hexane / 1 h / -78 - 0 °C / Inert atmosphere

2.2: 0.17 h / -40 °C / Inert atmosphere

2.3: 42.08 h / -60 - -50 °C / Inert atmosphere

3.1: 2,6-dimethylpyridine / dichloromethane / 4.58 h / 0 - 23 °C / Inert atmosphere

4.1: tetra-(n-butyl)ammonium iodide; potassium hydride / N,N-dimethyl-formamide / 24.08 h / 23 - 100 °C / Inert atmosphere

With 2,6-dimethylpyridine; 2,2,6,6-tetramethylpiperidinyl-lithium; tetra-(n-butyl)ammonium iodide; potassium hydride; lithium chloride; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201200387

Reference yield:

: 1380213-64-8
C₂₂H₂₆ClNO₂

: 1380213-66-0
C₄₇H₅₉ClN₄O₆SSi

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium chloride; lithium diisopropyl amide / tetrahydrofuran; hexane / 1 h / -78 - 0 °C / Inert atmosphere

1.2: 0.17 h / -40 °C / Inert atmosphere

1.3: 42.08 h / -60 - -50 °C / Inert atmosphere

2.1: 2,6-dimethylpyridine / dichloromethane / 4.58 h / 0 - 23 °C / Inert atmosphere

3.1: tetra-(n-butyl)ammonium iodide; potassium hydride / N,N-dimethyl-formamide / 24.08 h / 23 - 100 °C / Inert atmosphere

With 2,6-dimethylpyridine; tetra-(n-butyl)ammonium iodide; potassium hydride; lithium chloride; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201200387