methyl 2,6-anhydro-5-O-benzyl-7,8,9-trideoxy-D-glycero-L-galacto-non-8-enonate

Base Information

Chemical Name:methyl 2,6-anhydro-5-O-benzyl-7,8,9-trideoxy-D-glycero-L-galacto-non-8-enonate
CAS No.:866922-71-6
Molecular Formula:C₁₇H₂₂O₆
Molecular Weight:322.358
Hs Code.:

Synonyms:methyl 2,6-anhydro-5-O-benzyl-7,8,9-trideoxy-D-glycero-L-galacto-non-8-enonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2,6-anhydro-5-O-benzyl-7,8,9-trideoxy-D-glycero-L-galacto-non-8-enonate

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Technology Process of methyl 2,6-anhydro-5-O-benzyl-7,8,9-trideoxy-D-glycero-L-galacto-non-8-enonate

There total 13 articles about methyl 2,6-anhydro-5-O-benzyl-7,8,9-trideoxy-D-glycero-L-galacto-non-8-enonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 866922-60-3
methyl 2,6-anhydro-5-O-benzyl-3,4-O-isopropylidene-7,8,9-trideoxy-D-glycero-L-galacto-non-8-enolate

: 866922-71-6
methyl 2,6-anhydro-5-O-benzyl-7,8,9-trideoxy-D-glycero-L-galacto-non-8-enonate

Guidance literature:: With acetic acid; trifluoroacetic acid; In water; at 20 ℃; for 7h;

Reference yield: 81.0%

: 866922-67-0
methyl 3,4-di-O-acetyl-2,6-anhydro-5-O-benzyl-7,8,9-trideoxy-D-glycero-L-galacto-non-8-enonate

: 866922-71-6
methyl 2,6-anhydro-5-O-benzyl-7,8,9-trideoxy-D-glycero-L-galacto-non-8-enonate

Guidance literature:: With hydrogenchloride; In methanol; at 20 ℃; for 12h;

Reference yield:

: 866922-47-6
methyl 3,4,5-tri-O-acetyl-2,6-anhydro-7,8,9-trideoxy-D-glycero-L-galacto-non-8-enoate

: 866922-71-6
methyl 2,6-anhydro-5-O-benzyl-7,8,9-trideoxy-D-glycero-L-galacto-non-8-enonate

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / acetyl chloride; methanol / 19 h / 20 °C

2: 85 percent / p-toluenesulfonic acid monohydrate / benzene / 4.5 h / 20 °C

3: 70 percent / silver oxide / benzene / 28 h / 20 °C

4: 95 percent / acetic acid; trifluoroacetic acid / H₂O / 7 h / 20 °C

With methanol; toluene-4-sulfonic acid; acetic acid; acetyl chloride; trifluoroacetic acid; silver(l) oxide; In water; benzene;