methyl 2,6-anhydro-5-O-benzyl-3,4-O-isopropylidene-7,8,9-trideoxy-D-glycero-L-galacto-non-8-enolate

Base Information

Chemical Name:methyl 2,6-anhydro-5-O-benzyl-3,4-O-isopropylidene-7,8,9-trideoxy-D-glycero-L-galacto-non-8-enolate
CAS No.:866922-60-3
Molecular Formula:C₂₀H₂₆O₆
Molecular Weight:362.423
Hs Code.:

Synonyms:methyl 2,6-anhydro-5-O-benzyl-3,4-O-isopropylidene-7,8,9-trideoxy-D-glycero-L-galacto-non-8-enolate

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Chemical Property of methyl 2,6-anhydro-5-O-benzyl-3,4-O-isopropylidene-7,8,9-trideoxy-D-glycero-L-galacto-non-8-enolate

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Technology Process of methyl 2,6-anhydro-5-O-benzyl-3,4-O-isopropylidene-7,8,9-trideoxy-D-glycero-L-galacto-non-8-enolate

There total 9 articles about methyl 2,6-anhydro-5-O-benzyl-3,4-O-isopropylidene-7,8,9-trideoxy-D-glycero-L-galacto-non-8-enolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 866922-57-8
methyl 2,6-anhydro-3,4-O-isopropylidene-7,8,9-trideoxy-D-glycero-L-galacto-non-8-enonate

: 100-39-0
benzyl bromide

: 866922-60-3
methyl 2,6-anhydro-5-O-benzyl-3,4-O-isopropylidene-7,8,9-trideoxy-D-glycero-L-galacto-non-8-enolate

Guidance literature:: With silver(l) oxide; In benzene; at 20 ℃; for 28h;

Reference yield:

: 866922-47-6
methyl 3,4,5-tri-O-acetyl-2,6-anhydro-7,8,9-trideoxy-D-glycero-L-galacto-non-8-enoate

: 866922-60-3
methyl 2,6-anhydro-5-O-benzyl-3,4-O-isopropylidene-7,8,9-trideoxy-D-glycero-L-galacto-non-8-enolate

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / acetyl chloride; methanol / 19 h / 20 °C

2: 85 percent / p-toluenesulfonic acid monohydrate / benzene / 4.5 h / 20 °C

3: 70 percent / silver oxide / benzene / 28 h / 20 °C

With methanol; toluene-4-sulfonic acid; acetyl chloride; silver(l) oxide; In benzene;

Reference yield:

: (2S,3R,4R,5S,6R)-3,4,5-Triacetoxy-6-allyl-tetrahydro-pyran-2-carboxylic acid

: 866922-60-3
methyl 2,6-anhydro-5-O-benzyl-3,4-O-isopropylidene-7,8,9-trideoxy-D-glycero-L-galacto-non-8-enolate

Guidance literature:: Multi-step reaction with 4 steps

1: 130 mg / diethyl ether; CH₂Cl₂

2: 92 percent / acetyl chloride; methanol / 19 h / 20 °C

3: 85 percent / p-toluenesulfonic acid monohydrate / benzene / 4.5 h / 20 °C

4: 70 percent / silver oxide / benzene / 28 h / 20 °C

With methanol; toluene-4-sulfonic acid; acetyl chloride; silver(l) oxide; In diethyl ether; dichloromethane; benzene;