N-Butyl-N-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-4-hydroxy-benzamide

Base Information

Chemical Name:N-Butyl-N-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-4-hydroxy-benzamide
CAS No.:80764-62-1
Molecular Formula:C₃₃H₄₁N₃O₈
Molecular Weight:607.704
Hs Code.:

Synonyms:N-Butyl-N-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-4-hydroxy-benzamide

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Chemical Property of N-Butyl-N-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-4-hydroxy-benzamide

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Technology Process of N-Butyl-N-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-4-hydroxy-benzamide

There total 4 articles about N-Butyl-N-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-4-hydroxy-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53408-96-1
4'-nitrobenzo-18-crown-6

: 80764-62-1
N-Butyl-N-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-4-hydroxy-benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / Pd-C

2: 1.) NaNO₂, aq. HCl / 2.) room temperature, 1 d

3: Et₃N / tetrahydrofuran / 3 h / Ambient temperature

4: N₂H₄*H₂O / methanol / 0.5 h / Ambient temperature

With hydrogenchloride; hydrogen; hydrazine hydrate; triethylamine; sodium nitrite; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1021/ja00371a028

Reference yield:

: 81327-91-5
Acetic acid 4-{butyl-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-carbamoyl}-phenyl ester

: 80764-62-1
N-Butyl-N-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-4-hydroxy-benzamide

Guidance literature:: With hydrazine hydrate; In methanol; for 0.5h; Yield given; Ambient temperature;
DOI:10.1021/ja00371a028

Reference yield:

: 27914-73-4
4-acetoxybenzoyl chloride

: 80764-62-1
N-Butyl-N-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-4-hydroxy-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / tetrahydrofuran / 3 h / Ambient temperature

2: N₂H₄*H₂O / methanol / 0.5 h / Ambient temperature

With hydrazine hydrate; triethylamine; In tetrahydrofuran; methanol;
DOI:10.1021/ja00371a028