Butyl-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-amine

Base Information

• Chemical Name: Butyl-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-amine
• CAS No.: 80764-58-5
• Molecular Formula: C₂₆H₃₇N₃O₆
• Molecular Weight: 487.596

Synonyms:Butyl-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-amine

Chemical Property of Butyl-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-amine

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Technology Process of Butyl-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-amine

There total 2 articles about Butyl-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4'-nitrobenzo-18-crown-6 (53408-96-1) → Butyl-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-amine (80764-58-5)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂ / Pd-C

2: 1.) NaNO₂, aq. HCl / 2.) room temperature, 1 d

With hydrogenchloride; hydrogen; sodium nitrite; palladium on activated charcoal;

DOI:10.1021/ja00371a028

Reference yield:

N-(n-butyl)aniline (1126-78-9) + 4-aminobenzo-18-crown-6 (68941-06-0) → Butyl-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-amine (80764-58-5)

Guidance literature:

With hydrogenchloride; sodium nitrite; Yield given. Multistep reaction; 2.) room temperature, 1 d;

DOI:10.1021/ja00371a028

Reference yield: 17.0%

5-nitrosalicyloyl chloride (3223-20-9) + Butyl-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-amine (80764-58-5) → N-Butyl-N-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-2-hydroxy-5-nitro-benzamide (80780-59-2)

Guidance literature:

With sodium hydrogencarbonate; In tetrahydrofuran; Ambient temperature;

DOI:10.1021/ja00371a028

upstream raw materials:

N-(n-butyl)aniline

4-aminobenzo-18-crown-6

4'-nitrobenzo-18-crown-6

Downstream raw materials:

Acetic acid 4-{butyl-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-carbamoyl}-phenyl ester

N-Butyl-N-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-2-hydroxy-5-nitro-benzamide

Acetic acid 3-{butyl-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-carbamoyl}-phenyl ester

N-Butyl-N-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-3-hydroxy-benzamide

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