2-[2-(3-Methoxy-bicyclo[4.2.0]octa-1,3,5-trien-7-yl)-ethyl]-3-[(Z)-(S)-3-(1-methoxy-1-methyl-ethoxy)-5-phenyl-pent-1-enyl]-cyclopentanone

Base Information

Chemical Name:2-[2-(3-Methoxy-bicyclo[4.2.0]octa-1,3,5-trien-7-yl)-ethyl]-3-[(Z)-(S)-3-(1-methoxy-1-methyl-ethoxy)-5-phenyl-pent-1-enyl]-cyclopentanone
CAS No.:110560-43-5
Molecular Formula:C₃₁H₄₀O₄
Molecular Weight:476.656
Hs Code.:

Synonyms:2-[2-(3-Methoxy-bicyclo[4.2.0]octa-1,3,5-trien-7-yl)-ethyl]-3-[(Z)-(S)-3-(1-methoxy-1-methyl-ethoxy)-5-phenyl-pent-1-enyl]-cyclopentanone

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Chemical Property of 2-[2-(3-Methoxy-bicyclo[4.2.0]octa-1,3,5-trien-7-yl)-ethyl]-3-[(Z)-(S)-3-(1-methoxy-1-methyl-ethoxy)-5-phenyl-pent-1-enyl]-cyclopentanone

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Technology Process of 2-[2-(3-Methoxy-bicyclo[4.2.0]octa-1,3,5-trien-7-yl)-ethyl]-3-[(Z)-(S)-3-(1-methoxy-1-methyl-ethoxy)-5-phenyl-pent-1-enyl]-cyclopentanone

There total 1 articles about 2-[2-(3-Methoxy-bicyclo[4.2.0]octa-1,3,5-trien-7-yl)-ethyl]-3-[(Z)-(S)-3-(1-methoxy-1-methyl-ethoxy)-5-phenyl-pent-1-enyl]-cyclopentanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110560-34-4
2-[2-(3-Methoxy-bicyclo[4.2.0]octa-1,3,5-trien-7-yl)-ethyl]-cyclopent-2-enone

: C₁₅H₂₁CuO₂^(1-)*C₁₂H₂₇P*Li⁽¹⁺⁾

: 110560-43-5
2-[2-(3-Methoxy-bicyclo[4.2.0]octa-1,3,5-trien-7-yl)-ethyl]-3-[(Z)-(S)-3-(1-methoxy-1-methyl-ethoxy)-5-phenyl-pent-1-enyl]-cyclopentanone

Guidance literature:: at -70 ℃; for 2h;
DOI:10.1016/S0040-4039(00)89052-8

Reference yield:

: 110560-43-5
2-[2-(3-Methoxy-bicyclo[4.2.0]octa-1,3,5-trien-7-yl)-ethyl]-3-[(Z)-(S)-3-(1-methoxy-1-methyl-ethoxy)-5-phenyl-pent-1-enyl]-cyclopentanone

: 1624-62-0
estrone 3-methyl ether

Guidance literature:: Multi-step reaction with 5 steps

1: hexamethylphosphoric acid triamide / -30 °C

2: H⁽¹⁺⁾

3: OsO₄, NaIO₄ / pyridine

4: tetrahydrofuran / 0 °C

5: 70 percent / 1,2-dichloro-benzene / 180 °C

With sodium periodate; osmium(VIII) oxide; hydrogen cation; In tetrahydrofuran; pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; 1,2-dichloro-benzene;
DOI:10.1016/S0040-4039(00)89052-8