2-amino-9-(2-{4-[1-(tert-butyldimethylsilanyloxy)-4,4,5,5-tetramethyl-3-(1-methyl-1-trimethylsilanylethoxy)-imidazolidin-2-yl]-phenoxy}ethyl)-1,9-dihydro-purin-6-one

Base Information

Chemical Name:2-amino-9-(2-{4-[1-(tert-butyldimethylsilanyloxy)-4,4,5,5-tetramethyl-3-(1-methyl-1-trimethylsilanylethoxy)-imidazolidin-2-yl]-phenoxy}ethyl)-1,9-dihydro-purin-6-one
CAS No.:945594-49-0
Molecular Formula:C₃₂H₅₅N₇O₄Si₂
Molecular Weight:658.004
Hs Code.:

2-amino-9-(2-{4-[1-(tert-butyldimethylsilanyloxy)-4,4,5,5-tetramethyl-3-(1-methyl-1-trimethylsilanylethoxy)-imidazolidin-2-yl]-phenoxy}ethyl)-1,9-dihydro-purin-6-one

Synonyms:2-amino-9-(2-{4-[1-(tert-butyldimethylsilanyloxy)-4,4,5,5-tetramethyl-3-(1-methyl-1-trimethylsilanylethoxy)-imidazolidin-2-yl]-phenoxy}ethyl)-1,9-dihydro-purin-6-one

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Chemical Property of 2-amino-9-(2-{4-[1-(tert-butyldimethylsilanyloxy)-4,4,5,5-tetramethyl-3-(1-methyl-1-trimethylsilanylethoxy)-imidazolidin-2-yl]-phenoxy}ethyl)-1,9-dihydro-purin-6-one

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Technology Process of 2-amino-9-(2-{4-[1-(tert-butyldimethylsilanyloxy)-4,4,5,5-tetramethyl-3-(1-methyl-1-trimethylsilanylethoxy)-imidazolidin-2-yl]-phenoxy}ethyl)-1,9-dihydro-purin-6-one

There total 4 articles about 2-amino-9-(2-{4-[1-(tert-butyldimethylsilanyloxy)-4,4,5,5-tetramethyl-3-(1-methyl-1-trimethylsilanylethoxy)-imidazolidin-2-yl]-phenoxy}ethyl)-1,9-dihydro-purin-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 945594-48-9
9-(2-{4-[1-(tert-butyldimethylsilanyloxy)-4,4,5,5-tetramethyl-3-(1-methyl-1-trimethylsilanylethoxy)-imidazolidin-2-yl]-phenoxy}-ethyl)-6-methoxy-9H-purin-2-ylamine

: 945594-49-0
2-amino-9-(2-{4-[1-(tert-butyldimethylsilanyloxy)-4,4,5,5-tetramethyl-3-(1-methyl-1-trimethylsilanylethoxy)-imidazolidin-2-yl]-phenoxy}ethyl)-1,9-dihydro-purin-6-one

Guidance literature:: With trimethylsilyl iodide; In N,N-dimethyl-formamide; acetonitrile; at 20 ℃; for 23h;
DOI:10.1039/b702606d

Reference yield:

: 945594-45-6
2-[4-(2-bromoethoxy)phenyl]-4,4,5,5-tetramethylimidazolidine-1,3-diol

: 945594-49-0
2-amino-9-(2-{4-[1-(tert-butyldimethylsilanyloxy)-4,4,5,5-tetramethyl-3-(1-methyl-1-trimethylsilanylethoxy)-imidazolidin-2-yl]-phenoxy}ethyl)-1,9-dihydro-purin-6-one

Guidance literature:: Multi-step reaction with 4 steps

1: 1.71 g / imidazole / dimethylformamide / 29 h / 50 °C

2: 60.3 percent / K₂CO₃; KI / dimethylformamide / 25 h / 60 °C

3: methanol; CH₂Cl₂ / 0.58 h / 20 °C

4: 318.2 mg / Me₃SiI / dimethylformamide; acetonitrile / 23 h / 20 °C

With 1H-imidazole; trimethylsilyl iodide; potassium carbonate; potassium iodide; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/b702606d

Reference yield:

: 14384-45-3
N,N'-dihydroxy-2,3-dimethylbutane-2,3-diamine

: 945594-49-0
2-amino-9-(2-{4-[1-(tert-butyldimethylsilanyloxy)-4,4,5,5-tetramethyl-3-(1-methyl-1-trimethylsilanylethoxy)-imidazolidin-2-yl]-phenoxy}ethyl)-1,9-dihydro-purin-6-one

Guidance literature:: Multi-step reaction with 5 steps

1: benzene / 23 h / Heating

2: 1.71 g / imidazole / dimethylformamide / 29 h / 50 °C

3: 60.3 percent / K₂CO₃; KI / dimethylformamide / 25 h / 60 °C

4: methanol; CH₂Cl₂ / 0.58 h / 20 °C

5: 318.2 mg / Me₃SiI / dimethylformamide; acetonitrile / 23 h / 20 °C

With 1H-imidazole; trimethylsilyl iodide; potassium carbonate; potassium iodide; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; benzene;
DOI:10.1039/b702606d