4-(4-methylphenyl)-2,6-pyridinedicarbaldehyde

Base Information

Chemical Name:4-(4-methylphenyl)-2,6-pyridinedicarbaldehyde
CAS No.:717124-15-7
Molecular Formula:C₁₄H₁₁NO₂
Molecular Weight:225.247
Hs Code.:

Synonyms:4-(4-methylphenyl)-2,6-pyridinedicarbaldehyde

Suppliers and Price of 4-(4-methylphenyl)-2,6-pyridinedicarbaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-(4-methylphenyl)-2,6-pyridinedicarbaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-(4-methylphenyl)-2,6-pyridinedicarbaldehyde

There total 3 articles about 4-(4-methylphenyl)-2,6-pyridinedicarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1422463-82-8
4-(4-methylphenyl)-2,6-bis(1-pyrrolidinylcarbonyl)pyridine

: 717124-15-7
4-(4-methylphenyl)-2,6-pyridinedicarbaldehyde

Guidance literature:: 4-(4-methylphenyl)-2,6-bis(1-pyrrolidinylcarbonyl)pyridine; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 1h;

With hydrogenchloride; In tetrahydrofuran; water;
DOI:10.1016/j.tetlet.2012.11.004

Reference yield:

: 120491-93-2
4-bromopyridine-2,6-dicarbonyl dibromide

: 717124-15-7
4-(4-methylphenyl)-2,6-pyridinedicarbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 2 h / 0 - 20 °C

2: potassium carbonate; palladium diacetate; triphenylphosphine / water; 1,2-dimethoxyethane / 2 h / Inert atmosphere; Reflux

3: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C

With lithium aluminium tetrahydride; palladium diacetate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water;
DOI:10.1016/j.tetlet.2012.11.004

Reference yield:

: 1422463-81-7
4-bromo-2,6-bis(1-pyrrolidinylcarbonyl)pyridine

: 717124-15-7
4-(4-methylphenyl)-2,6-pyridinedicarbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; palladium diacetate; triphenylphosphine / water; 1,2-dimethoxyethane / 2 h / Inert atmosphere; Reflux

2: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C

With lithium aluminium tetrahydride; palladium diacetate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; 1,2-dimethoxyethane; water;
DOI:10.1016/j.tetlet.2012.11.004