C₄₈H₉₀O₄Si₂

Base Information

Chemical Name:C₄₈H₉₀O₄Si₂
CAS No.:1412439-03-2
Molecular Formula:C₄₈H₉₀O₄Si₂
Molecular Weight:787.411
Hs Code.:

C<sub>48</sub>H<sub>90</sub>O<sub>4</sub>Si<sub>2</sub>

Synonyms:C₄₈H₉₀O₄Si₂

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Chemical Property of C₄₈H₉₀O₄Si₂

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Technology Process of C₄₈H₉₀O₄Si₂

There total 6 articles about C₄₈H₉₀O₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1412438-97-1
7-((3R,3aR,4R,7S,7aR)-octahydro-3-[(1S)-2-iodo-1-methylethyl]-3a-methyl-1H-indene-4-yl)-α,α-dimethylheptanol

: 1412439-03-2
C₄₈H₉₀O₄Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: pyridine; zinc; nickel(II) chloride hexahydrate / 2 h / 60 °C / Inert atmosphere

1.2: 0.33 h / 20 °C / Inert atmosphere

2.1: Dess-Martin periodane / dichloromethane / 1 h / Inert atmosphere; Darkness

3.1: tetrahydrofuran; toluene / 5 h / -17 - 20 °C / Inert atmosphere

4.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; tricyclohexylphosphine; potassium acetate / dimethyl sulfoxide / 3 h / 80 °C / Inert atmosphere

5.1: potassium phosphate; bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 1 h / Inert atmosphere; Darkness

5.2: Inert atmosphere

6.1: diethyl ether / 1.25 h / -78 - 20 °C / Inert atmosphere; Darkness

With pyridine; bis-triphenylphosphine-palladium(II) chloride; potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; nickel(II) chloride hexahydrate; potassium acetate; Dess-Martin periodane; zinc; tricyclohexylphosphine; In tetrahydrofuran; diethyl ether; dichloromethane; dimethyl sulfoxide; toluene; 3.1: |Wittig Olefination / 5.1: |Suzuki-Miyaura Coupling;
DOI:10.1002/hlca.201200427

Reference yield:

: 1412439-00-9
methyl (δR,1R,3aR,4E,7R,7aR)-4-(bromomethylene)octahydro-7-(7-hydroxy-7-methyloctyl)-δ,7a-dimethyl-1H-indene-1-pentanoate

: 1412439-03-2
C₄₈H₉₀O₄Si₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; tricyclohexylphosphine; potassium acetate / dimethyl sulfoxide / 3 h / 80 °C / Inert atmosphere

2.1: potassium phosphate; bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 1 h / Inert atmosphere; Darkness

2.2: Inert atmosphere

3.1: diethyl ether / 1.25 h / -78 - 20 °C / Inert atmosphere; Darkness

With bis-triphenylphosphine-palladium(II) chloride; potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; tricyclohexylphosphine; In tetrahydrofuran; diethyl ether; dimethyl sulfoxide; 2.1: |Suzuki-Miyaura Coupling;
DOI:10.1002/hlca.201200427

Reference yield:

: 1412438-98-2
methyl (δR,1R,3aR,4S,7R,7aR)-octahydro-4-hydroxy-7-(7-hydroxy-7-methyloctyl)-δ,7a-dimethyl-1H-indene-1-pentanoate

: 1412439-03-2
C₄₈H₉₀O₄Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: Dess-Martin periodane / dichloromethane / 1 h / Inert atmosphere; Darkness

2.1: tetrahydrofuran; toluene / 5 h / -17 - 20 °C / Inert atmosphere

3.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; tricyclohexylphosphine; potassium acetate / dimethyl sulfoxide / 3 h / 80 °C / Inert atmosphere

4.1: potassium phosphate; bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 1 h / Inert atmosphere; Darkness

4.2: Inert atmosphere

5.1: diethyl ether / 1.25 h / -78 - 20 °C / Inert atmosphere; Darkness

With bis-triphenylphosphine-palladium(II) chloride; potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; Dess-Martin periodane; tricyclohexylphosphine; In tetrahydrofuran; diethyl ether; dichloromethane; dimethyl sulfoxide; toluene; 2.1: |Wittig Olefination / 4.1: |Suzuki-Miyaura Coupling;
DOI:10.1002/hlca.201200427