O-[3-(1,3-benzothiazol-2-yl)phenyl]diphenylthiophosphinate

Base Information

• Chemical Name: O-[3-(1,3-benzothiazol-2-yl)phenyl]diphenylthiophosphinate
• CAS No.: 1305316-85-1
• Molecular Formula: C₂₅H₁₈NOPS₂
• Molecular Weight: 443.53
• Mol file: 1305316-85-1.mol

Synonyms:O-[3-(1,3-benzothiazol-2-yl)phenyl]diphenylthiophosphinate

Chemical Property of O-[3-(1,3-benzothiazol-2-yl)phenyl]diphenylthiophosphinate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of O-[3-(1,3-benzothiazol-2-yl)phenyl]diphenylthiophosphinate

There total 5 articles about O-[3-(1,3-benzothiazol-2-yl)phenyl]diphenylthiophosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

3-benzothiazol-2-yl-phenol (25389-28-0) + diphenylthiophosphinoyl chloride (1015-37-8) → O-[3-(1,3-benzothiazol-2-yl)phenyl]diphenylthiophosphinate (1305316-85-1)

Guidance literature:

With triethylamine; In benzene; at 60 ℃;

DOI:10.1021/om101012r

Reference yield:

3-methoxy-N-phenylbenzenecarbothioamide → O-[3-(1,3-benzothiazol-2-yl)phenyl]diphenylthiophosphinate (1305316-85-1)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydroxide; potassium hexacyanoferrate(III)

2: triethylamine / benzene / 2 h / 60 °C

With triethylamine; sodium hydroxide; potassium hexacyanoferrate(III); In benzene;

DOI:10.1080/10426507.2010.507726

Reference yield:

phenyl isothiocyanate (103-72-0) → O-[3-(1,3-benzothiazol-2-yl)phenyl]diphenylthiophosphinate (1305316-85-1)

Guidance literature:

Multi-step reaction with 3 steps

1: magnesium

2: sodium hydroxide; potassium hexacyanoferrate(III)

3: triethylamine / benzene / 2 h / 60 °C

With magnesium; triethylamine; sodium hydroxide; potassium hexacyanoferrate(III); In benzene;

DOI:10.1080/10426507.2010.507726

upstream raw materials:

3-methoxyphenyl bromide

3-benzothiazol-2-yl-phenol

diphenylthiophosphinoyl chloride

phenyl isothiocyanate

Downstream raw materials:

{2-(1,3-benzothiazol-2-yl)-6-[(diphenylthiophosphoryl)oxy]phenyl}palladium chloride