1-(2-hydroxyethyl)-12-{2-[(2-phenyl-1,3-dioxan-4-yl)methoxy]ethyl}-1,12-dicarba-closo-dodecaborane

Base Information

Chemical Name:1-(2-hydroxyethyl)-12-{2-[(2-phenyl-1,3-dioxan-4-yl)methoxy]ethyl}-1,12-dicarba-closo-dodecaborane
CAS No.:1566526-77-9
Molecular Formula:C₁₇H₃₂B₁₀O₄
Molecular Weight:408.549
Hs Code.:

Synonyms:1-(2-hydroxyethyl)-12-{2-[(2-phenyl-1,3-dioxan-4-yl)methoxy]ethyl}-1,12-dicarba-closo-dodecaborane

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Chemical Property of 1-(2-hydroxyethyl)-12-{2-[(2-phenyl-1,3-dioxan-4-yl)methoxy]ethyl}-1,12-dicarba-closo-dodecaborane

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Technology Process of 1-(2-hydroxyethyl)-12-{2-[(2-phenyl-1,3-dioxan-4-yl)methoxy]ethyl}-1,12-dicarba-closo-dodecaborane

There total 1 articles about 1-(2-hydroxyethyl)-12-{2-[(2-phenyl-1,3-dioxan-4-yl)methoxy]ethyl}-1,12-dicarba-closo-dodecaborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 35918-13-9
1,12-bis(2-hydroxyethyl)-1,12-dicarba-closo-dodecaborane

: 127945-31-7
4-(p-toluenesulfonyloxymethyl)-2-phenyl-1,3-dioxane

: 1566526-77-9
1-(2-hydroxyethyl)-12-{2-[(2-phenyl-1,3-dioxan-4-yl)methoxy]ethyl}-1,12-dicarba-closo-dodecaborane

Guidance literature:: 1,12-bis(2-hydroxyethyl)-1,12-dicarba-closo-dodecaborane; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.166667h;

4-(p-toluenesulfonyloxymethyl)-2-phenyl-1,3-dioxane; In N,N-dimethyl-formamide; at 20 ℃; for 18h;
DOI:10.1016/j.bmc.2014.01.015

Reference yield: 36.0%

: 1566526-77-9
1-(2-hydroxyethyl)-12-{2-[(2-phenyl-1,3-dioxan-4-yl)methoxy]ethyl}-1,12-dicarba-closo-dodecaborane

: 105-36-2
ethyl bromoacetate

: 1566526-78-0
1-{2-[(2-phenyl-1,3-dioxan-4-yl)methoxy]ethyl}-12-[2-(ethoxycarbonylmethoxy)ethyl]-1,12-dicarba-closo-dodecaborane

Guidance literature:: 1-(2-hydroxyethyl)-12-{2-[(2-phenyl-1,3-dioxan-4-yl)methoxy]ethyl}-1,12-dicarba-closo-dodecaborane; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.166667h;

ethyl bromoacetate; at 20 ℃; for 18h;
DOI:10.1016/j.bmc.2014.01.015

Reference yield: 17.0%

: 13547-70-1
1-chloro-3,3-dimethyl-butan-2-one

: 1566526-77-9
1-(2-hydroxyethyl)-12-{2-[(2-phenyl-1,3-dioxan-4-yl)methoxy]ethyl}-1,12-dicarba-closo-dodecaborane

: 1566526-80-4
1-{2-[(2-phenyl-1,3-dioxan-4-yl)methoxy]ethyl}-12-[2-(3,3-dimethyl-2-oxobutoxy)ethyl]-1,12-dicarba-closo-dodecaborane

Guidance literature:: 1-(2-hydroxyethyl)-12-{2-[(2-phenyl-1,3-dioxan-4-yl)methoxy]ethyl}-1,12-dicarba-closo-dodecaborane; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.166667h;

1-chloro-3,3-dimethyl-butan-2-one; at 20 ℃; for 18h;
DOI:10.1016/j.bmc.2014.01.015