1,1-dimethylethyl 2-(2-cyano-9-methyl-9H-purin-6-yl)-2-cyclo-hexyl-hydrazine-carboxylate

Base Information

Chemical Name:1,1-dimethylethyl 2-(2-cyano-9-methyl-9H-purin-6-yl)-2-cyclo-hexyl-hydrazine-carboxylate
CAS No.:1055926-74-3
Molecular Formula:C₁₈H₂₅N₇O₂
Molecular Weight:371.442
Hs Code.:

Synonyms:1,1-dimethylethyl 2-(2-cyano-9-methyl-9H-purin-6-yl)-2-cyclo-hexyl-hydrazine-carboxylate

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Chemical Property of 1,1-dimethylethyl 2-(2-cyano-9-methyl-9H-purin-6-yl)-2-cyclo-hexyl-hydrazine-carboxylate

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Technology Process of 1,1-dimethylethyl 2-(2-cyano-9-methyl-9H-purin-6-yl)-2-cyclo-hexyl-hydrazine-carboxylate

There total 3 articles about 1,1-dimethylethyl 2-(2-cyano-9-methyl-9H-purin-6-yl)-2-cyclo-hexyl-hydrazine-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1055926-73-2
1,1-dimethylethyl 2-(2-chloro-9-methyl-9H-purin-6-yl)-2-cyclo-hexyl-hydrazine-carboxylate

: 557-21-1
dicyanozinc

: 1055926-74-3
1,1-dimethylethyl 2-(2-cyano-9-methyl-9H-purin-6-yl)-2-cyclo-hexyl-hydrazine-carboxylate

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; zinc; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In ISOPROPYLAMIDE; at 150 ℃; for 0.0833333h; under 9000.9 Torr; Microwave irradiation;

Reference yield:

: 2382-10-7
2,6-dichloro-9-methyl-9H-purine

: 1055926-74-3
1,1-dimethylethyl 2-(2-cyano-9-methyl-9H-purin-6-yl)-2-cyclo-hexyl-hydrazine-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 48 h / Heating / reflux

2: 1,1'-bis-(diphenylphosphino)ferrocene; zinc / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / ISOPROPYLAMIDE / 0.08 h / 150 °C / 9000.9 Torr / Microwave irradiation

With 1,1'-bis-(diphenylphosphino)ferrocene; N-ethyl-N,N-diisopropylamine; zinc; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In ISOPROPYLAMIDE; isopropyl alcohol;

Reference yield:

: 5451-40-1
2,6-dichloropurine

: 1055926-74-3
1,1-dimethylethyl 2-(2-cyano-9-methyl-9H-purin-6-yl)-2-cyclo-hexyl-hydrazine-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / dimethyl sulfoxide / 20 °C

2: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 48 h / Heating / reflux

3: 1,1'-bis-(diphenylphosphino)ferrocene; zinc / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / ISOPROPYLAMIDE / 0.08 h / 150 °C / 9000.9 Torr / Microwave irradiation

With 1,1'-bis-(diphenylphosphino)ferrocene; potassium carbonate; N-ethyl-N,N-diisopropylamine; zinc; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In ISOPROPYLAMIDE; dimethyl sulfoxide; isopropyl alcohol;