acetyl 6-O-benzoyl-3,4-di-O-isopropylidene-2-deoxy-2-iodo-β-D-galactoside

Base Information

• Chemical Name: acetyl 6-O-benzoyl-3,4-di-O-isopropylidene-2-deoxy-2-iodo-β-D-galactoside
• CAS No.: 548460-00-0
• Molecular Formula: C₁₈H₂₁IO₇
• Molecular Weight: 476.265

Synonyms:acetyl 6-O-benzoyl-3,4-di-O-isopropylidene-2-deoxy-2-iodo-β-D-galactoside

Chemical Property of acetyl 6-O-benzoyl-3,4-di-O-isopropylidene-2-deoxy-2-iodo-β-D-galactoside

Chemical Property:

Purity/Quality:

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Technology Process of acetyl 6-O-benzoyl-3,4-di-O-isopropylidene-2-deoxy-2-iodo-β-D-galactoside

There total 1 articles about acetyl 6-O-benzoyl-3,4-di-O-isopropylidene-2-deoxy-2-iodo-β-D-galactoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

acetic acid (64-19-7,77671-22-8) + 6-O-benzoyl-3,4-di-O-isopropylidene-D-galactal (172360-80-4) → acetyl 6-O-benzoyl-3,4-di-O-isopropylidene-2-deoxy-2-iodo-β-D-galactoside (548460-00-0) + acetyl 6-O-benzoyl-3,4-di-O-isopropylidene-2-deoxy-2-iodo-α-D-galactoside

Guidance literature:

With N-iodo-succinimide; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1021/ol034393t

Reference yield:

methyl 2,3,4-tri-O-benzoylglucopyranoside (34234-44-1) + acetyl 6-O-benzoyl-3,4-di-O-isopropylidene-2-deoxy-2-iodo-β-D-galactoside (548460-00-0) → methyl 2,3,4-tribenzoyl-6-O-(6-O-benzoyl-3,4-di-O-isopropylidene-2-deoxy-2-iodo-β-D-galactopyranosyl)-(1->3)-α-D-glucopyranoside + methyl 2,3,4-tribenzoyl-6-O-(6-O-benzoyl-3,4-di-O-isopropylidene-2-deoxy-2-iodo-α-D-galactopyranosyl)-(1->3)-α-D-glucopyranoside

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃;

DOI:10.1021/ol034393t

Reference yield:

acetyl 6-O-benzoyl-3,4-di-O-isopropylidene-2-deoxy-2-iodo-β-D-galactoside (548460-00-0) + methyl 2-O-benzoyl-4,6-di-O-benzylidene-α-D-glucopyranoside (28642-64-0,35823-97-3,38992-99-3,51591-23-2,55169-75-0,56253-26-0,72659-78-0,80041-30-1,80299-59-8,86420-70-4,86420-72-6,91685-06-2,99265-94-8,109010-33-5,118246-05-2,126255-07-0) → methyl 4,6-benzylidene-2-O-benzoyl-3-O-(6-O-benzoyl-3,4-di-O-isopropylidene-2-deoxy-2-iodo-β-D-galactopyranosyl)-(1->3)-α-D-glucopyranoside + methyl 4,6-benzylidene-2-O-benzoyl-3-O-(6-O-benzoyl-3,4-di-O-isopropylidene-2-deoxy-2-iodo-α-D-galactopyranosyl)-(1->3)-α-D-glucopyranoside

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃;

DOI:10.1021/ol034393t

upstream raw materials:

acetic acid

6-O-benzoyl-3,4-di-O-isopropylidene-D-galactal

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