1-<2-<(4-nitrophenoxy)carbonyl>benzyl>-3-(aminocarbonyl)quinolinium bromide

Base Information

Chemical Name:1-<2-<(4-nitrophenoxy)carbonyl>benzyl>-3-(aminocarbonyl)quinolinium bromide
CAS No.:117593-67-6
Molecular Formula:Br*C₂₄H₁₈N₃O₅
Molecular Weight:508.328
Hs Code.:

Synonyms:1-<2-<(4-nitrophenoxy)carbonyl>benzyl>-3-(aminocarbonyl)quinolinium bromide

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Chemical Property of 1-<2-<(4-nitrophenoxy)carbonyl>benzyl>-3-(aminocarbonyl)quinolinium bromide

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Technology Process of 1-<2-<(4-nitrophenoxy)carbonyl>benzyl>-3-(aminocarbonyl)quinolinium bromide

There total 4 articles about 1-<2-<(4-nitrophenoxy)carbonyl>benzyl>-3-(aminocarbonyl)quinolinium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 6480-67-7
quinoline-3-carboxamide

: 79251-23-3
α-bromo-p-nitrophenyl o-toluate

: 117593-67-6
1-<2-<(4-nitrophenoxy)carbonyl>benzyl>-3-(aminocarbonyl)quinolinium bromide

Guidance literature:: In tetrahydrofuran; for 12h; Heating;
DOI:10.1016/S0040-4020(01)86744-2

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 117593-67-6
1-<2-<(4-nitrophenoxy)carbonyl>benzyl>-3-(aminocarbonyl)quinolinium bromide

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / pyridine / diethyl ether / 2 h

2: N-bromosuccinimide, benzoylperoxide / various solvent(s) / 12 h / Heating

3: 76 percent / tetrahydrofuran / 12 h / Heating

With pyridine; N-Bromosuccinimide; Perbenzoic acid; In tetrahydrofuran; diethyl ether;
DOI:10.1016/S0040-4020(01)86744-2

Reference yield:

: 74738-56-0
4-nitrophenyl 2-methylbenzoate

: 117593-67-6
1-<2-<(4-nitrophenoxy)carbonyl>benzyl>-3-(aminocarbonyl)quinolinium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: N-bromosuccinimide, benzoylperoxide / various solvent(s) / 12 h / Heating

2: 76 percent / tetrahydrofuran / 12 h / Heating

With N-Bromosuccinimide; Perbenzoic acid; In tetrahydrofuran;
DOI:10.1016/S0040-4020(01)86744-2