C₃₂H₅₁PS

Base Information

Chemical Name:C₃₂H₅₁PS
CAS No.:1417613-55-8
Molecular Formula:C₃₂H₅₁PS
Molecular Weight:498.797
Hs Code.:

Synonyms:C₃₂H₅₁PS

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₂H₅₁PS

Chemical Property:

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Technology Process of C₃₂H₅₁PS

There total 3 articles about C₃₂H₅₁PS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1417613-52-5
C₃₂H₅₁P

: 1417613-55-8
C₃₂H₅₁PS

Guidance literature:: With S₈; triethylamine; In toluene; at 20 ℃; for 1.5h; Reflux; Inert atmosphere;
DOI:10.1039/c2dt31971c

Reference yield:

: 3975-77-7
1-bromo-2,4,6-tri-tert-butylbenzene

: 1417613-55-8
C₃₂H₅₁PS

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C

2.1: chloro-trimethyl-silane; lithium aluminium tetrahydride / 1,4-dioxane / 5 h / 100 °C / Inert atmosphere

3.1: triethylamine; S₈ / toluene / 1.5 h / 20 °C / Reflux; Inert atmosphere

With lithium aluminium tetrahydride; n-butyllithium; chloro-trimethyl-silane; S₈; triethylamine; In tetrahydrofuran; 1,4-dioxane; hexane; toluene;
DOI:10.1039/c2dt31971c

Reference yield:

: 73557-52-5
bis(2,4,6-tris(1,1-dimethylethyl)phenyl)phosphinic chloride

: 1417613-55-8
C₃₂H₅₁PS

Guidance literature:: Multi-step reaction with 2 steps

1: chloro-trimethyl-silane; lithium aluminium tetrahydride / 1,4-dioxane / 5 h / 100 °C / Inert atmosphere

2: triethylamine; S₈ / toluene / 1.5 h / 20 °C / Reflux; Inert atmosphere

With lithium aluminium tetrahydride; chloro-trimethyl-silane; S₈; triethylamine; In 1,4-dioxane; toluene;
DOI:10.1039/c2dt31971c