sodium 2-(2-hydroxy-5-(pyridin-4-yl)benzamido)-4-(2-methoxyphenyl)benzoic acid

Base Information

Chemical Name:sodium 2-(2-hydroxy-5-(pyridin-4-yl)benzamido)-4-(2-methoxyphenyl)benzoic acid
CAS No.:1237514-72-5
Molecular Formula:C₂₆H₁₉N₂O₅*Na
Molecular Weight:462.437
Hs Code.:

Synonyms:sodium 2-(2-hydroxy-5-(pyridin-4-yl)benzamido)-4-(2-methoxyphenyl)benzoic acid

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Chemical Property of sodium 2-(2-hydroxy-5-(pyridin-4-yl)benzamido)-4-(2-methoxyphenyl)benzoic acid

Chemical Property:

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Technology Process of sodium 2-(2-hydroxy-5-(pyridin-4-yl)benzamido)-4-(2-methoxyphenyl)benzoic acid

There total 12 articles about sodium 2-(2-hydroxy-5-(pyridin-4-yl)benzamido)-4-(2-methoxyphenyl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1237519-21-9
2-(2-hydroxy-5-(pyridin-4-yl)benzamido)-4-(2-methoxyphenyl)benzoic acid

: 1237514-72-5
sodium 2-(2-hydroxy-5-(pyridin-4-yl)benzamido)-4-(2-methoxyphenyl)benzoic acid

Guidance literature:: With sodium hydroxide; In 1,4-dioxane; water; at 20 ℃; for 2.5h;

Reference yield:

: 1237517-77-9
2-[(phenylmethyl)oxy]-5-(4-pyridinyl)benzoic acid

: 1237514-72-5
sodium 2-(2-hydroxy-5-(pyridin-4-yl)benzamido)-4-(2-methoxyphenyl)benzoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 2.5 h / 20 °C

2: pyridine / dichloromethane / 2 h / 20 °C / Cooling with ice

3: hydrogen / palladium 10% on activated carbon / ethyl acetate; 1,4-dioxane; methanol / 6 h / 20 °C

4: trifluoroacetic acid / 1.5 h / 20 °C

5: sodium hydroxide / 1,4-dioxane; water / 2.5 h / 20 °C

With pyridine; oxalyl dichloride; hydrogen; trifluoroacetic acid; sodium hydroxide; palladium 10% on activated carbon; N,N-dimethyl-formamide; In 1,4-dioxane; methanol; dichloromethane; water; ethyl acetate;

Reference yield:

: 1237519-19-5
tert-butyl 2-(2-(benzyloxy)-5-(pyridin-4-yl)benzamido)-4-(2-methoxyphenyl)benzoate

: 1237514-72-5
sodium 2-(2-hydroxy-5-(pyridin-4-yl)benzamido)-4-(2-methoxyphenyl)benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / palladium 10% on activated carbon / ethyl acetate; 1,4-dioxane; methanol / 6 h / 20 °C

2: trifluoroacetic acid / 1.5 h / 20 °C

3: sodium hydroxide / 1,4-dioxane; water / 2.5 h / 20 °C

With hydrogen; trifluoroacetic acid; sodium hydroxide; palladium 10% on activated carbon; In 1,4-dioxane; methanol; water; ethyl acetate;