tert-butyl 2-(2-hydroxy-5-(pyridin-4-yl)benzamido)-4-(2-methoxyphenyl)benzoate

Base Information

Chemical Name:tert-butyl 2-(2-hydroxy-5-(pyridin-4-yl)benzamido)-4-(2-methoxyphenyl)benzoate
CAS No.:1237519-20-8
Molecular Formula:C₃₀H₂₈N₂O₅
Molecular Weight:496.563
Hs Code.:

Synonyms:tert-butyl 2-(2-hydroxy-5-(pyridin-4-yl)benzamido)-4-(2-methoxyphenyl)benzoate

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Chemical Property of tert-butyl 2-(2-hydroxy-5-(pyridin-4-yl)benzamido)-4-(2-methoxyphenyl)benzoate

Chemical Property:

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Technology Process of tert-butyl 2-(2-hydroxy-5-(pyridin-4-yl)benzamido)-4-(2-methoxyphenyl)benzoate

There total 10 articles about tert-butyl 2-(2-hydroxy-5-(pyridin-4-yl)benzamido)-4-(2-methoxyphenyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1237519-19-5
tert-butyl 2-(2-(benzyloxy)-5-(pyridin-4-yl)benzamido)-4-(2-methoxyphenyl)benzoate

: 1237519-20-8
tert-butyl 2-(2-hydroxy-5-(pyridin-4-yl)benzamido)-4-(2-methoxyphenyl)benzoate

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In 1,4-dioxane; methanol; ethyl acetate; at 20 ℃; for 6h;

Reference yield:

: 1237517-77-9
2-[(phenylmethyl)oxy]-5-(4-pyridinyl)benzoic acid

: 1237519-20-8
tert-butyl 2-(2-hydroxy-5-(pyridin-4-yl)benzamido)-4-(2-methoxyphenyl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 2.5 h / 20 °C

2: pyridine / dichloromethane / 2 h / 20 °C / Cooling with ice

3: hydrogen / palladium 10% on activated carbon / ethyl acetate; 1,4-dioxane; methanol / 6 h / 20 °C

With pyridine; oxalyl dichloride; hydrogen; palladium 10% on activated carbon; N,N-dimethyl-formamide; In 1,4-dioxane; methanol; dichloromethane; ethyl acetate;

Reference yield:

: 2-(benzyloxy)-5-(pyridin-4-yl)benzoic acid chloride

: 1237519-20-8
tert-butyl 2-(2-hydroxy-5-(pyridin-4-yl)benzamido)-4-(2-methoxyphenyl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 2 h / 20 °C / Cooling with ice

2: hydrogen / palladium 10% on activated carbon / ethyl acetate; 1,4-dioxane; methanol / 6 h / 20 °C

With pyridine; hydrogen; palladium 10% on activated carbon; In 1,4-dioxane; methanol; dichloromethane; ethyl acetate;