C₄₇H₆₉NO₇

Base Information

Chemical Name:C₄₇H₆₉NO₇
CAS No.:1370547-52-6
Molecular Formula:C₄₇H₆₉NO₇
Molecular Weight:760.067
Hs Code.:

C<sub>47</sub>H<sub>69</sub>NO<sub>7</sub>

Synonyms:C₄₇H₆₉NO₇

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Chemical Property of C₄₇H₆₉NO₇

Chemical Property:

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Technology Process of C₄₇H₆₉NO₇

There total 12 articles about C₄₇H₆₉NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1370547-50-4
(1S,2R,3R,4aR,6aS,7R,8R,10aR,10bR,12aR)-3-acetoxy-2-((S)-2-(((benzyloxy)carbonyl)(methyl)amino)-2,3-dimethylbutoxy)-1,6a,8,10a-tetramethyl-8-((R)-3-methylbutan-2-yl)-2,3,4,6,6a,7,8,9,10,10a,10b,11,12,12a-tetradecahydro-1H-1,4a-(methanooxymethano)chrysene-7-carboxylic acid

: 1370547-52-6
C₄₇H₆₉NO₇

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 35 ℃; Large scale reaction;
DOI:10.1021/jo300046v

Reference yield:

: 952577-51-4
(S)-2-ethoxycarbonylamino-2,3-dimethylbutyric acid

: 1370547-52-6
C₄₇H₆₉NO₇

Guidance literature:: Multi-step reaction with 9 steps

1: lithium aluminium tetrahydride / tetrahydrofuran; 2-methyltetrahydrofuran / 60 °C / Large scale reaction

2: thionyl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane / -17 - -3 °C / Large scale reaction

3: sodium periodate; rhodium(III) chloride hydrate / acetonitrile / 20 °C / Large scale reaction

4: potassium 2-methylbutan-2-olate / N,N-dimethyl acetamide; toluene / 24.5 h / 20 - 25 °C / Large scale reaction

5: toluene-4-sulfonic acid; acetic acid / Isopropyl acetate / 3.5 h / 20 - 60 °C / Large scale reaction

6: palladium 10% on activated carbon; formic acid; triethylamine / tetrahydrofuran / 0.5 h / 50 °C / Large scale reaction

7: potassium carbonate / tetrahydrofuran; toluene / 3 h / 20 °C

8: sodium hydroxide / 6 h / 20 °C / Large scale reaction

9: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 35 °C / Large scale reaction

With sodium periodate; lithium aluminium tetrahydride; formic acid; thionyl chloride; rhodium(III) chloride hydrate; palladium 10% on activated carbon; potassium 2-methylbutan-2-olate; potassium carbonate; toluene-4-sulfonic acid; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; 2-methyltetrahydrofuran; dichloromethane; N,N-dimethyl acetamide; Isopropyl acetate; toluene; acetonitrile;
DOI:10.1021/jo300046v

Reference yield:

: 1370547-49-1
(1S,2R,3R,4aR,6aS,7R,8R,10aR,10bR,12aR)-3-acetoxy-2-((S)-2,3-dimethyl-2-(methylamino)butoxy)-1,6a,8,10a-tetramethyl-8-((R)-3-methylbutan-2-yl)-2,3,4,6,6a,7,8,9,10,10a,10b,-11,12,12a-tetradecahydro-1H-1,4a-(methanooxymethano)-chrysene-7-carboxylic acid

: 1370547-52-6
C₄₇H₆₉NO₇

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / tetrahydrofuran; toluene / 3 h / 20 °C

2: sodium hydroxide / 6 h / 20 °C / Large scale reaction

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 35 °C / Large scale reaction

With potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/jo300046v