Methyl 4,4,4-trifluoro-3--2-(methoxycarbonyl)-2-butenoate

Base Information

Chemical Name:Methyl 4,4,4-trifluoro-3--2-(methoxycarbonyl)-2-butenoate
CAS No.:944583-09-9
Molecular Formula:C₁₅H₁₆F₃NO₆
Molecular Weight:363.29
Hs Code.:

Methyl 4,4,4-trifluoro-3-<N-(2,4-dimethoxyphenyl)amino>-2-(methoxycarbonyl)-2-butenoate

Synonyms:Methyl 4,4,4-trifluoro-3--2-(methoxycarbonyl)-2-butenoate

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Chemical Property of Methyl 4,4,4-trifluoro-3--2-(methoxycarbonyl)-2-butenoate

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Technology Process of Methyl 4,4,4-trifluoro-3--2-(methoxycarbonyl)-2-butenoate

There total 1 articles about Methyl 4,4,4-trifluoro-3--2-(methoxycarbonyl)-2-butenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: N-(2,4-Dimethoxy-phenyl)-2,2,2-trifluoro-acetimidoyl chloride

: 108-59-8
malonic acid dimethyl ester

: 944583-09-9
Methyl 4,4,4-trifluoro-3--2-(methoxycarbonyl)-2-butenoate

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 4h; Ambient temperature;
DOI:10.1021/jo00086a053

Reference yield: 64.0%

: 944583-09-9
Methyl 4,4,4-trifluoro-3--2-(methoxycarbonyl)-2-butenoate

: Methyl 4,4,4-trifluoro-3--2-(methoxycarbonyl)-2-butenoate

Guidance literature:: In water; acetonitrile; at -10 ℃; electrolyse: undivided cell, glassy carbon anode, platinum cathode, 5mA/cm² for 2.5 F/mol of electricity, NaHCO₃;
DOI:10.1021/jo00086a053