Technology Process of C11H9F3N2O
There total 4 articles about C11H9F3N2O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
iron; ammonium chloride;
In
ethanol; water;
at 80 ℃;
for 1h;
Product distribution / selectivity;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: ammonium cerium(IV) nitrate / N,N-dimethyl-formamide / 4 h / 0 - 20 °C
2: water; iron; ammonium chloride / ethanol / 0.83 h / 100 - 105 °C
With
ammonium cerium(IV) nitrate; water; iron; ammonium chloride;
In
ethanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N-ethyl-N,N-diisopropylamine / 1-methylpiperidin-2-one / -10 - 20 °C
2: triethylamine / tetrahydrofuran / 2.67 h / 0 - 20 °C
3: ammonium cerium(IV) nitrate / N,N-dimethyl-formamide / 4 h / 0 - 20 °C
4: water; iron; ammonium chloride / ethanol / 0.83 h / 100 - 105 °C
With
ammonium cerium(IV) nitrate; water; iron; ammonium chloride; triethylamine; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; 1-methylpiperidin-2-one; ethanol; N,N-dimethyl-formamide;