(E)-4-methyl-N'-(1-(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydronaphthalen-2-yl)ethylidene)benzenesulfonohydrazide

Base Information

Chemical Name:(E)-4-methyl-N'-(1-(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydronaphthalen-2-yl)ethylidene)benzenesulfonohydrazide
CAS No.:1417652-27-7
Molecular Formula:C₂₄H₃₂N₂O₂S
Molecular Weight:412.596
Hs Code.:

Synonyms:(E)-4-methyl-N'-(1-(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydronaphthalen-2-yl)ethylidene)benzenesulfonohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-4-methyl-N'-(1-(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydronaphthalen-2-yl)ethylidene)benzenesulfonohydrazide

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Technology Process of (E)-4-methyl-N'-(1-(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydronaphthalen-2-yl)ethylidene)benzenesulfonohydrazide

There total 1 articles about (E)-4-methyl-N'-(1-(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydronaphthalen-2-yl)ethylidene)benzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 17610-24-1
1-(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydronaphthalenyl)ethanone

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 1417652-27-7
(E)-4-methyl-N'-(1-(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydronaphthalen-2-yl)ethylidene)benzenesulfonohydrazide

Guidance literature:: In methanol; at 60 ℃;
DOI:10.1021/jo3023268

Reference yield: 76.0%

: 696-62-8
para-iodoanisole

: 1417652-27-7
(E)-4-methyl-N'-(1-(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydronaphthalen-2-yl)ethylidene)benzenesulfonohydrazide

: 1417652-45-9
6-(1-(4-methoxyphenyl)vinyl)-1,1,4,4,7-pentamethyl-1,2,3,4-tetrahydronaphthalene

Guidance literature:: With dichloro bis(acetonitrile) palladium(II); sodium t-butanolate; XPhos; In fluorobenzene; at 100 ℃; for 2h; Sealed tube;
DOI:10.1021/jo3023268