(E)-3-[5-(1,2-dimethyl-2-propenyl)-4-hydroxy-3-methoxyphenyl]-1-(2,4,6-trihydroxyphenyl)-2-propen-1-one

Base Information

Chemical Name:(E)-3-[5-(1,2-dimethyl-2-propenyl)-4-hydroxy-3-methoxyphenyl]-1-(2,4,6-trihydroxyphenyl)-2-propen-1-one
CAS No.:1412939-09-3
Molecular Formula:C₂₁H₂₂O₆
Molecular Weight:370.402
Hs Code.:

Synonyms:(E)-3-[5-(1,2-dimethyl-2-propenyl)-4-hydroxy-3-methoxyphenyl]-1-(2,4,6-trihydroxyphenyl)-2-propen-1-one

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Chemical Property of (E)-3-[5-(1,2-dimethyl-2-propenyl)-4-hydroxy-3-methoxyphenyl]-1-(2,4,6-trihydroxyphenyl)-2-propen-1-one

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Technology Process of (E)-3-[5-(1,2-dimethyl-2-propenyl)-4-hydroxy-3-methoxyphenyl]-1-(2,4,6-trihydroxyphenyl)-2-propen-1-one

There total 5 articles about (E)-3-[5-(1,2-dimethyl-2-propenyl)-4-hydroxy-3-methoxyphenyl]-1-(2,4,6-trihydroxyphenyl)-2-propen-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: C₂₃H₂₆O₇

: 1412939-09-3
(E)-3-[5-(1,2-dimethyl-2-propenyl)-4-hydroxy-3-methoxyphenyl]-1-(2,4,6-trihydroxyphenyl)-2-propen-1-one

Guidance literature:: With hydrogenchloride; water; In methanol; at 35 ℃;
DOI:10.1007/s00044-012-0282-9

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 1412939-09-3
(E)-3-[5-(1,2-dimethyl-2-propenyl)-4-hydroxy-3-methoxyphenyl]-1-(2,4,6-trihydroxyphenyl)-2-propen-1-one

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / acetone / 20 °C

2: N,N-dimethyl-aniline / 26 h / 185 °C / Inert atmosphere; Sealed tube

3: potassium carbonate / acetone / 12 h

4: potassium hydroxide / ethanol; water / Inert atmosphere; Cooling with ice

5: hydrogenchloride; water / methanol / 35 °C

With hydrogenchloride; water; potassium carbonate; N,N-dimethyl-aniline; potassium hydroxide; In methanol; ethanol; water; acetone; 2: |Claisen Rearrangement / 4: |Claisen-Schmidt Condensation;
DOI:10.1007/s00044-012-0282-9

Reference yield:

: 39953-41-8
3-methoxy-4-[(3-methylbut-2-en-1-yl)oxy] benzaldehyde

: 1412939-09-3
(E)-3-[5-(1,2-dimethyl-2-propenyl)-4-hydroxy-3-methoxyphenyl]-1-(2,4,6-trihydroxyphenyl)-2-propen-1-one

Guidance literature:: Multi-step reaction with 4 steps

1: N,N-dimethyl-aniline / 26 h / 185 °C / Inert atmosphere; Sealed tube

2: potassium carbonate / acetone / 12 h

3: potassium hydroxide / ethanol; water / Inert atmosphere; Cooling with ice

4: hydrogenchloride; water / methanol / 35 °C

With hydrogenchloride; water; potassium carbonate; N,N-dimethyl-aniline; potassium hydroxide; In methanol; ethanol; water; acetone; 1: |Claisen Rearrangement / 3: |Claisen-Schmidt Condensation;
DOI:10.1007/s00044-012-0282-9